Measurement of lateral and axial resolution of confocal Raman microscope using dispersed carbon nanotubes and suspended graphene

• Published in: Current applied physics 2020, 20(1), , pp.71-77
• Main Authors: Kim, Youngbum, Lee, Eun Ji, Roy, Shrawan, Sharbirin, Anir S., Ranz, Lars-Gunnar, Dieing, Thomas, Kim, Jeongyong
• Format: Article
• Language: English
• Subjects: FWHM; Raman mapping; Raman spectroscopy; Rayleigh criterion; Resolution; 물리학
• ISSN: 1567-1739; 1878-1675
• DOI: 10.1016/j.cap.2019.10.012

A confocal Raman microscope (CRM) facilitates visualization of the spatial distribution of molecular bonds or phonon modes at the submicron level and has been extensively used in the characterization of nanomaterials and devices. The lateral and axial resolution is a key specification that defines the performance of CRM, however, the interpretation of spatial resolution in the literature is often ambiguous, making it often difficult to directly compare Raman images obtained under different conditions. In this report, a convenient and reliable measurement protocol using dispersed carbon nanotubes and suspended graphene as test specimens is proposed to facilitate the determination of the lateral and axial resolutions of a CRM. Spatial resolution values comparable to the results based on Rayleigh criterion calculations were obtained using Raman mapping images of test specimens. This was achieved without the need for complex deconvolution processes or the consideration of an asymmetric dielectric environment. [Display omitted] •Protocol to measure spatial resolution of confocal Raman microscope was provided.•Test specimens were prepared by dispersed carbon nanotubes and suspended graphene.•Resolutions comparable to Rayleigh criterion was obtained without deconvolution.•Our procedure provides reference to assess performance of confocal Raman microscope.