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Quantitative analysis of the size distributions and elements of the precipitates in Fe-3%Si alloy during secondary recrystallization annealing using HAADF imaging and XEDS

The distribution of precipitates on grain boundaries and their role in abnormal grain growth during secondary recrystallization annealing in Fe-3 %Si alloy is studied. The precipitates and grain boundaries were observed simultaneously using high angle annular dark field scanning transmission electro...

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Bibliographic Details
Published in:Metals and materials international 2009, 15(1), , pp.113-118
Main Authors: Yim, Jung-Ryoul, Min, Ah-Ri, Joo, Young-Chang
Format: Article
Language:English
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Summary:The distribution of precipitates on grain boundaries and their role in abnormal grain growth during secondary recrystallization annealing in Fe-3 %Si alloy is studied. The precipitates and grain boundaries were observed simultaneously using high angle annular dark field scanning transmission electron microscopy. The chemical composition of the precipitates was also analyzed by X-ray energy dispersive spectroscopy. During secondary recrystallization annealing, the number of small precipitates (
ISSN:1598-9623
2005-4149
DOI:10.1007/s12540-009-0113-9