Production of bio-epoxide and bio-adhesive from non-edible oil

Epoxidation of Nahor oil was performed by H 2 O 2 in the presence of acid catalyst at 50 °C. It was possible to obtain around 70% epoxide yield within 8 hrs of reaction. Amberlite IR 120H showed better epoxide yield compared to H 2 SO 4 and Dowex 50 WX8. The performance of carboxylic acids was found...

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Bibliographic Details
Published in:The Korean journal of chemical engineering 2016, 33(10), 199, pp.2915-2922
Main Authors: Dinda, Srikanta, Veeram, Nikhil Sainath Reddy, Adusumalli, Ramesh Babu
Format: Article
Language:English
Subjects:
Acetic acid
Acids
Adhesion tests
Amberlite (trademark)
Biotechnology
Carboxylic acids
Cardboard
Catalysis
Chemistry
Chemistry and Materials Science
Epoxidation
Ethylenediamine
Formic acid
Hydrogen peroxide
Industrial Chemistry/Chemical Engineering
Materials Science
Propionic acid
Sulfuric acid
화학공학
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Summary:Epoxidation of Nahor oil was performed by H 2 O 2 in the presence of acid catalyst at 50 °C. It was possible to obtain around 70% epoxide yield within 8 hrs of reaction. Amberlite IR 120H showed better epoxide yield compared to H 2 SO 4 and Dowex 50 WX8. The performance of carboxylic acids was found to be in the order of formic acid>acetic acid>propanoic acid. The curing of epoxidized nahor oil involved using ethylenediamine (EDA) and diethylenetriamine (DETA). The adhesive property of the cured resins was tested and compared with commercially available glue. The force required to detach the cardboard joint was about 36.3 N for DETA-cured resin.
ISSN:0256-1115
1975-7220
DOI:10.1007/s11814-016-0136-0