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Analysis of the Structural Evolution of Zinc Oxide Powders Obtained by Mechanical High-Energy Grinding
Zinc oxide powders made by mechanical high-energy grinding have been investigated using the methods of scanning electron microscopy, thermal nitrogen desorption, and Raman spectroscopy of infrared Fourier spectroscopy. Their structural evolution, including reduction of the average size of crystallit...
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| Published in: | Technical physics 2019-09, Vol.64 (9), p.1330-1335 |
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| Main Authors: | , , , , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c459t-3c87aacb8d74a30df8256ca58e5e3486f1690429fee775350daa39f44240a2ed3 |
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| cites | cdi_FETCH-LOGICAL-c459t-3c87aacb8d74a30df8256ca58e5e3486f1690429fee775350daa39f44240a2ed3 |
| container_end_page | 1335 |
| container_issue | 9 |
| container_start_page | 1330 |
| container_title | Technical physics |
| container_volume | 64 |
| creator | Averin, I. A. Pronin, I. A. Yakushova, N. D. Karmanov, A. A. Sychev, M. M. Vikhman, S. V. Levitsky, V. S. Moshnikov, V. A. Terukov, E. I. |
| description | Zinc oxide powders made by mechanical high-energy grinding have been investigated using the methods of scanning electron microscopy, thermal nitrogen desorption, and Raman spectroscopy of infrared Fourier spectroscopy. Their structural evolution, including reduction of the average size of crystallites, increase in specific surface area, as well as changes in the number and ratio of adsorption centers, has been demonstrated. The data on the reconstruction of the surface of zinc oxide powders and multiple bond breaking in near-surface areas resulting from long-term dispersion have been presented. |
| doi_str_mv | 10.1134/S1063784219090020 |
| format | article |
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A. ; Pronin, I. A. ; Yakushova, N. D. ; Karmanov, A. A. ; Sychev, M. M. ; Vikhman, S. V. ; Levitsky, V. S. ; Moshnikov, V. A. ; Terukov, E. I.</creator><creatorcontrib>Averin, I. A. ; Pronin, I. A. ; Yakushova, N. D. ; Karmanov, A. A. ; Sychev, M. M. ; Vikhman, S. V. ; Levitsky, V. S. ; Moshnikov, V. A. ; Terukov, E. I.</creatorcontrib><description>Zinc oxide powders made by mechanical high-energy grinding have been investigated using the methods of scanning electron microscopy, thermal nitrogen desorption, and Raman spectroscopy of infrared Fourier spectroscopy. Their structural evolution, including reduction of the average size of crystallites, increase in specific surface area, as well as changes in the number and ratio of adsorption centers, has been demonstrated. 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| ispartof | Technical physics, 2019-09, Vol.64 (9), p.1330-1335 |
| issn | 1063-7842 1090-6525 |
| language | eng |
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| source | Springer Nature |
| subjects | ADSORPTION Classical and Continuum Physics CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY Crystallites DESORPTION Evolution FOURIER TRANSFORM SPECTROMETERS GRINDING INFRARED SPECTRA NITROGEN Physics Physics and Astronomy Physics of Nanostructures POWDERS RAMAN SPECTROSCOPY SCANNING ELECTRON MICROSCOPY SPECIFIC SURFACE AREA Spectrum analysis SURFACE AREA Zinc oxide ZINC OXIDES |
| title | Analysis of the Structural Evolution of Zinc Oxide Powders Obtained by Mechanical High-Energy Grinding |
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