Synthesis of Single-Crystal Barium Titanium Isopropoxide Complex to Form Barium Titanate

Single‐crystal barium titanate double alkoxide complex with a composition presumed to be BaTi(OCH(CH3)2)6·xC6H6 was successfully synthesized in this work. The crystal was converted to BaTiO3 at 100°C. The preparation of the Oxides via single crystals of metal alkoxides has some advantages over the w...

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Bibliographic Details
Published in:Journal of the American Ceramic Society 1994-02, Vol.77 (2), p.603-605
Main Authors: Suyama, Yoko, Nagasawa, Mitsuru
Format: Article
Language:English
Subjects:
360201 - Ceramics, Cermets, & Refractories- Preparation & Fabrication
360202 - Ceramics, Cermets, & Refractories- Structure & Phase Studies
ALKALINE EARTH METAL COMPOUNDS
BARIUM COMPOUNDS
BARIUM OXIDES
CHALCOGENIDES
Chemistry
CRYSTAL GROWTH
Exact sciences and technology
FABRICATION
Inorganic chemistry and origins of life
MATERIALS SCIENCE
OXIDES
OXYGEN COMPOUNDS
Preparations and properties
Salts
STOICHIOMETRY
TITANIUM COMPOUNDS
TITANIUM OXIDES
TRANSITION ELEMENT COMPOUNDS
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Summary:Single‐crystal barium titanate double alkoxide complex with a composition presumed to be BaTi(OCH(CH3)2)6·xC6H6 was successfully synthesized in this work. The crystal was converted to BaTiO3 at 100°C. The preparation of the Oxides via single crystals of metal alkoxides has some advantages over the well‐known sol‐gel method in that it results in oxides with well‐defined and homogeneous compositions at the atomic level and in fine particle sizes, smaller than 50 nm.
ISSN:0002-7820
1551-2916
DOI:10.1111/j.1151-2916.1994.tb07037.x