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Electron backscatter diffraction analysis of Nb3Al multifilamentary strands prepared by rapid heating, quenching and transformation annealing
To enhance the non-Cu critical current density Jc at 15 T and 4.2 K (1000 A mm - 2 at present) we have endeavoured to refine the grain size of rapid heating, quenching and transformation (RHQT)-processed Nb3Al. In the present study, the grain boundary structures of RHQT-processed Nb3Al were examined...
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Published in: | Superconductor science & technology 2010-12, Vol.23 (12), p.125001-125001 |
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creator | Takeuchi, T Tsuchiya, K Saeda, M Banno, N Kikuchi, A Iijima, Y |
description | To enhance the non-Cu critical current density Jc at 15 T and 4.2 K (1000 A mm - 2 at present) we have endeavoured to refine the grain size of rapid heating, quenching and transformation (RHQT)-processed Nb3Al. In the present study, the grain boundary structures of RHQT-processed Nb3Al were examined by electron backscatter diffraction (EBSD) because transgranular fracture prevents the observation of fractured cross sections of Nb3Al to statistically determine the grain size. The grain size distributions of body-centred-cubic supersaturated-solid-solution Nb(Al)ss and A15 Nb3Al filaments were measured for grains misoriented by more than 2 degree , 5 degree and 15 degree . A mixed grain structure, which consists of a few large grains (>25 mu m) and many small grains ( |
doi_str_mv | 10.1088/0953-2048/23/12/125001 |
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In the present study, the grain boundary structures of RHQT-processed Nb3Al were examined by electron backscatter diffraction (EBSD) because transgranular fracture prevents the observation of fractured cross sections of Nb3Al to statistically determine the grain size. The grain size distributions of body-centred-cubic supersaturated-solid-solution Nb(Al)ss and A15 Nb3Al filaments were measured for grains misoriented by more than 2 degree , 5 degree and 15 degree . A mixed grain structure, which consists of a few large grains (>25 mu m) and many small grains (<1 mu m), was observed for an Nb3Al filament that had been transformed from non-deformed Nb(Al)ss. Plastic deformation that had been made between the rapid heating and quenching steps and the transformation step apparently homogenized the grain size distribution and then reduced the average grain size. The misorientation angle distributions of Nb(Al)ss and Nb3Al were also measured and compared with each other. A clear relationship between the Jc and the inverse grain size was not confirmed for the RHQT Nb3Al conductors examined in the present study, which indicates the importance of making a filament compositionally homogeneous to obtain a high Jc.</description><identifier>ISSN: 0953-2048</identifier><identifier>EISSN: 1361-6668</identifier><identifier>DOI: 10.1088/0953-2048/23/12/125001</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>Applied sciences ; Electrical engineering. 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In the present study, the grain boundary structures of RHQT-processed Nb3Al were examined by electron backscatter diffraction (EBSD) because transgranular fracture prevents the observation of fractured cross sections of Nb3Al to statistically determine the grain size. The grain size distributions of body-centred-cubic supersaturated-solid-solution Nb(Al)ss and A15 Nb3Al filaments were measured for grains misoriented by more than 2 degree , 5 degree and 15 degree . A mixed grain structure, which consists of a few large grains (>25 mu m) and many small grains (<1 mu m), was observed for an Nb3Al filament that had been transformed from non-deformed Nb(Al)ss. Plastic deformation that had been made between the rapid heating and quenching steps and the transformation step apparently homogenized the grain size distribution and then reduced the average grain size. The misorientation angle distributions of Nb(Al)ss and Nb3Al were also measured and compared with each other. A clear relationship between the Jc and the inverse grain size was not confirmed for the RHQT Nb3Al conductors examined in the present study, which indicates the importance of making a filament compositionally homogeneous to obtain a high Jc.</description><subject>Applied sciences</subject><subject>Electrical engineering. Electrical power engineering</subject><subject>Electron back scatter diffraction</subject><subject>Exact sciences and technology</subject><subject>Filaments</subject><subject>Grain size</subject><subject>Grain size distribution</subject><subject>Grains</subject><subject>Heating</subject><subject>Materials</subject><subject>Quenching</subject><subject>Transformations</subject><issn>0953-2048</issn><issn>1361-6668</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNptkU1rGzEQhkVpoG6Sv1B0Kb10Y314tdpjMPkC016as5jVR61Wq91K8sE_Iv85WmxySUGgQfPMO5p3EPpCyQ0lUq5J3_KGkY1cM76mrJ6WEPoBrSgXtBFCyI9o9QZ9Qp9z_lMBKjlboZe7YHVJU8QD6L9ZQyk2YeOdS6CLr-8QIRyzz3hy-MfAbwMeD6F45wOMNhZIR5xLgmgynpOdIVmDhyNOMHuD9xaKj7-_438HG_W-hlXP4IXPbkojnFtEC6Emr9CFg5Dt9fm-RM_3d7-2j83u58PT9nbXeC54abQTnQYmtXSGUd5rYTpThwXO-FDDHvTGCWHalgnN2NCLoddtJyznZGMrdIm-nXTnNNWf5aJGn7UNAaKdDllJSYToeikr-fVMQjUnVFei9lnNyY91csV4SyjrFkV64vw0v2UpUcuG1GK-WsyvvKJMnTZUa5r3Nf9n1WwcfwWw25Ro</recordid><startdate>20101201</startdate><enddate>20101201</enddate><creator>Takeuchi, T</creator><creator>Tsuchiya, K</creator><creator>Saeda, M</creator><creator>Banno, N</creator><creator>Kikuchi, A</creator><creator>Iijima, Y</creator><general>IOP Publishing</general><general>Institute of Physics</general><scope>IQODW</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20101201</creationdate><title>Electron backscatter diffraction analysis of Nb3Al multifilamentary strands prepared by rapid heating, quenching and transformation annealing</title><author>Takeuchi, T ; Tsuchiya, K ; Saeda, M ; Banno, N ; Kikuchi, A ; Iijima, Y</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-i363t-cf67ca28c8fd2139c6d7d361a323bd7d9ac4f66d5526c22b96b9c576e3304e323</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Applied sciences</topic><topic>Electrical engineering. Electrical power engineering</topic><topic>Electron back scatter diffraction</topic><topic>Exact sciences and technology</topic><topic>Filaments</topic><topic>Grain size</topic><topic>Grain size distribution</topic><topic>Grains</topic><topic>Heating</topic><topic>Materials</topic><topic>Quenching</topic><topic>Transformations</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Takeuchi, T</creatorcontrib><creatorcontrib>Tsuchiya, K</creatorcontrib><creatorcontrib>Saeda, M</creatorcontrib><creatorcontrib>Banno, N</creatorcontrib><creatorcontrib>Kikuchi, A</creatorcontrib><creatorcontrib>Iijima, Y</creatorcontrib><collection>Pascal-Francis</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Superconductor science & technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Takeuchi, T</au><au>Tsuchiya, K</au><au>Saeda, M</au><au>Banno, N</au><au>Kikuchi, A</au><au>Iijima, Y</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Electron backscatter diffraction analysis of Nb3Al multifilamentary strands prepared by rapid heating, quenching and transformation annealing</atitle><jtitle>Superconductor science & technology</jtitle><date>2010-12-01</date><risdate>2010</risdate><volume>23</volume><issue>12</issue><spage>125001</spage><epage>125001</epage><pages>125001-125001</pages><issn>0953-2048</issn><eissn>1361-6668</eissn><abstract>To enhance the non-Cu critical current density Jc at 15 T and 4.2 K (1000 A mm - 2 at present) we have endeavoured to refine the grain size of rapid heating, quenching and transformation (RHQT)-processed Nb3Al. In the present study, the grain boundary structures of RHQT-processed Nb3Al were examined by electron backscatter diffraction (EBSD) because transgranular fracture prevents the observation of fractured cross sections of Nb3Al to statistically determine the grain size. The grain size distributions of body-centred-cubic supersaturated-solid-solution Nb(Al)ss and A15 Nb3Al filaments were measured for grains misoriented by more than 2 degree , 5 degree and 15 degree . A mixed grain structure, which consists of a few large grains (>25 mu m) and many small grains (<1 mu m), was observed for an Nb3Al filament that had been transformed from non-deformed Nb(Al)ss. Plastic deformation that had been made between the rapid heating and quenching steps and the transformation step apparently homogenized the grain size distribution and then reduced the average grain size. The misorientation angle distributions of Nb(Al)ss and Nb3Al were also measured and compared with each other. A clear relationship between the Jc and the inverse grain size was not confirmed for the RHQT Nb3Al conductors examined in the present study, which indicates the importance of making a filament compositionally homogeneous to obtain a high Jc.</abstract><cop>Bristol</cop><pub>IOP Publishing</pub><doi>10.1088/0953-2048/23/12/125001</doi><tpages>1</tpages></addata></record> |
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subjects | Applied sciences Electrical engineering. Electrical power engineering Electron back scatter diffraction Exact sciences and technology Filaments Grain size Grain size distribution Grains Heating Materials Quenching Transformations |
title | Electron backscatter diffraction analysis of Nb3Al multifilamentary strands prepared by rapid heating, quenching and transformation annealing |
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