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Isolation and Analysis of Essential Oils from Spices

Natural product isolation and analysis provide an opportunity to present a variety of experimental techniques to undergraduate students in introductory organic chemistry. Eugenol, anethole, and carvone were extracted from six common spices using steam-distillation and diethyl ether as the extraction...

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Bibliographic Details
Published in:Journal of chemical education 2012-04, Vol.89 (5), p.665-668
Main Authors: O’Shea, Stephen K, Von Riesen, Daniel D, Rossi, Lauren L
Format: Article
Language:English
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Summary:Natural product isolation and analysis provide an opportunity to present a variety of experimental techniques to undergraduate students in introductory organic chemistry. Eugenol, anethole, and carvone were extracted from six common spices using steam-distillation and diethyl ether as the extraction solvent. Students assessed the purity of their spice extract and identified its components via TLC, reverse-phase HPLC, and GC–MS analyses. In addition, students reviewed molecular characteristics and interactions while discovering the similarities and differences among the six spice extracts.
ISSN:0021-9584
1938-1328
DOI:10.1021/ed101141w