Preparation and Characterization of Mesoporous Al-MCM-41 Layers Deposited on FeCrAl Metallic Foils by an In-situ Hydrothermal Method

A new class of activated mesoporous Al-MCM-41 layers was deposited on Fe-CrAl metallic foils in the presence of cationic surfactant cetyltrimethylammonium bromide under basic conditions by an in-situ hydrothermal method. The characterization techniques including X-ray diffraction, nitrogen adsorptio...

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Published in:Journal of Wuhan University of Technology. Materials science edition 2009-02, Vol.24 (1), p.1-4
Main Authors: Wei, Qi, Liu, Li, Nie, Zuoren, Chen, Zengxiang, Zou, Jingxia
Format: Article
Language:English
Subjects:
Chemistry and Materials Science
Materials Science
MCM
Scanning electron microscopy
原位
水热法
沉积
溴化十六烷基三甲铵
表征技术
金属箔
阳离子表面活性剂
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cited_by cdi_FETCH-LOGICAL-c343t-5d2a9710cac0e30e5de2abf8f2da74ac33e3492a393478308f4ef98aae0335443
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container_title Journal of Wuhan University of Technology. Materials science edition
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creator Wei, Qi
Liu, Li
Nie, Zuoren
Chen, Zengxiang
Zou, Jingxia
description A new class of activated mesoporous Al-MCM-41 layers was deposited on Fe-CrAl metallic foils in the presence of cationic surfactant cetyltrimethylammonium bromide under basic conditions by an in-situ hydrothermal method. The characterization techniques including X-ray diffraction, nitrogen adsorption and transmission electron microscopy, as well as field-emission scanning electron microscopy were performed to investigate the pore structure and surface morphology of the Al-MCM-41 layers. The Al-MCM-41 materials are of amorphous structure but exhibit large BET surface area （up to 757.0 m2/g） and pore volume （up to 0.72 cm3/g）, as well as a mean pore diameter of 3 nm. The layers deposited on the FeCrAl foils are continuous despite with a few of holes on the surface.
doi_str_mv 10.1007/s11595-009-1001-3
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1993-0437
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source Springer Nature
subjects Chemistry and Materials Science
Materials Science
MCM
Scanning electron microscopy
原位
水热法
沉积
溴化十六烷基三甲铵
表征技术
金属箔
阳离子表面活性剂
title Preparation and Characterization of Mesoporous Al-MCM-41 Layers Deposited on FeCrAl Metallic Foils by an In-situ Hydrothermal Method
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