Residue of Organphosphorus Pesticides in Chewing Cane Juices Detected by QuEChERS and GC-NPD Method

• Published in: Plant Diseases and Pests(植物病虫害研究：英文版) 2013-08, Vol.4 (4), p.8-11
• Main Authors: Yegeng, Fan, Jie, Liao, Jun, Liang, Leixing, Mo, Tianshun, Wang, Yu, Ya, Qiang, Liang, Song, Li
• Format: Article
• Language: English
• Subjects: 农药残留测定; 快速分析方法; 有机磷农药; 果汁; 果蔗; 检测; 甲基毒死蜱; 相对标准偏差
• ISSN: 2152-3932

[ Objective] The paper was to establish a quick detection method for residue of organphosphoras pesticides in chewing cane juices and provide guarantee for edible safety of chewing juice. [ Method] By using QuEChERS and GC-NPD method, a rapid analysis method for residue of six kinds of organphosphorus pesti- cides （dichlorves, chlorpyrifos-methyl, malathion, fenthion, chlorpyrifos and triazophes） in sugarcane juices was established. [ Resdt] QuEChERS method was significantly superior to traditional extraction method and could extract six kinds of organphesphorus pesticides from chewing cane juices effectively, which gready saved organic reagent and time. Good linearity was found in different standard curves; when the concentration of pesticides was from 0. 020 toO. 100 rag/L, the re- covery rate was from 68.58% to 92.85%, and relative standard deviation （RSD） was ranged from 2.16% to 9.89%. [ Conclusion] The sensitivity, accuracy and precision of QuEChERS method were consistent with the technical requirements of pesticide residue determination. It not only could shorten sample processing cycle effectively, but also ensure that no impurity was in the sample peak and the recovery rate was also consistent with the requirements of residual analysis.