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Mechanism of the Gelation of Fibroin Solution

Degummed silk was dissolved in a mixture of CaCl 2 and ethanol at low temperature. The concentration and pH of the centrifuged, filtered, and dialyzed silk solution were adjusted, and then it was kept in an air-conditioned room for gelation. The mechanism of the gelation and the gel structure were s...

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Bibliographic Details
Published in:Bioscience, biotechnology, and biochemistry biotechnology, and biochemistry, 1993, Vol.57 (11), p.1910-1912
Main Authors: Ayub, Zuglul Haider, Arai, Mitsuo, Hirabayashi, Kiyoshi
Format: Article
Language:English
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Summary:Degummed silk was dissolved in a mixture of CaCl 2 and ethanol at low temperature. The concentration and pH of the centrifuged, filtered, and dialyzed silk solution were adjusted, and then it was kept in an air-conditioned room for gelation. The mechanism of the gelation and the gel structure were studied. It was found that the gel was formed due to the formation of beta-structure in the fibroin solution. The gelation was dependent on the pH of the fibroin solution.
ISSN:0916-8451
1347-6947
DOI:10.1271/bbb.57.1910