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Preparation of Calcium-Strontium Apatite through Mechanochemical Method

The formation of a calcium-strontium apatite solid solution precursor via mechanochemical method was described. The precursor is formed by a process of ball-milling of a slurry consisting of a mixture of the starting materials; CaHPO4·2H2O, CaCO3, SrHPO4 and Sr(OH)4·8H2O in a zirconia pot mill for 2...

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Bibliographic Details
Published in:Chemistry letters 1996-01, Vol.25 (1), p.91-92
Main Authors: Yokogawa, Yoshiyuki, Toriyama, Motohiro, Kawamoto, Yukari, Suzuki, Takahiro, Nishizawa, Kaori, Nagata, Fukue, Mucalo, M. R
Format: Article
Language:English
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Summary:The formation of a calcium-strontium apatite solid solution precursor via mechanochemical method was described. The precursor is formed by a process of ball-milling of a slurry consisting of a mixture of the starting materials; CaHPO4·2H2O, CaCO3, SrHPO4 and Sr(OH)4·8H2O in a zirconia pot mill for 24 h in the presence of water at room temperature over the entire Ca/(Ca+Sr) compositional range. Calcium-stontium apatite precursor obtained from ball-milling began to change to calcium-stontium apatite upon heating at temperature over 500 °C.
ISSN:0366-7022
1348-0715
DOI:10.1246/cl.1996.91