A Novel Route to Obtain Molybdenum Dichalcogenides by Hydrothermal Reaction

Hydrothermal reactions between aqueous Na2MoO4, Na2ESO3 (E = S, Se) and hydrazine monohydrate at 135 °C for 12 h produce phase-pure MoS2 and MoSe2 with good yield of about 90%. X-Ray powder diffraction, chemical analysis and X-ray photoelectron spectroscopy were used to characterize the structure an...

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Published in:Chemistry letters 2000-08, Vol.29 (8), p.920-921
Main Authors: Fan, Rong, Chen, Xianhui, Chen, Zuyao
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Language:English
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description Hydrothermal reactions between aqueous Na2MoO4, Na2ESO3 (E = S, Se) and hydrazine monohydrate at 135 °C for 12 h produce phase-pure MoS2 and MoSe2 with good yield of about 90%. X-Ray powder diffraction, chemical analysis and X-ray photoelectron spectroscopy were used to characterize the structure and composition of the products annealed at 350 °C. Transmission electron microscopy images show that the samples of MoS2 and MoSe2 consist of nano-crystallites with average particle size of 4 nm and 7 nm, respectively.
doi_str_mv 10.1246/cl.2000.920
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title A Novel Route to Obtain Molybdenum Dichalcogenides by Hydrothermal Reaction
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