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CAN/I2-catalyzed Chemoselective Synthesis of Thiosulfonates by Oxidation of Disulfides or Thiols

CAN/I2 promoted synthesis of thiosulfonates by oxidation of disulfides and thiols with high chemoselectivity and excellent yields in wet poly(ethylene glycol) (PEG-400). The overall process is simple, practical, and it provides convenient access to thiosulfonates.

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Bibliographic Details
Published in:Chemistry letters 2010-04, Vol.39 (4), p.368-369
Main Authors: Cai, Ming-Tiao, Lv, Guang-Shu, Chen, Jiu-Xi, Gao, Wen-Xia, Ding, Jin-Chang, Wu, Hua-Yue
Format: Article
Language:English
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Summary:CAN/I2 promoted synthesis of thiosulfonates by oxidation of disulfides and thiols with high chemoselectivity and excellent yields in wet poly(ethylene glycol) (PEG-400). The overall process is simple, practical, and it provides convenient access to thiosulfonates.
ISSN:0366-7022
1348-0715
DOI:10.1246/cl.2010.368