Convenient Synthesis of 3,5-Biscarbamoyl-pyridine Derivatives

An efficient and convenient method for synthesis of 3,5-bis-carbamoyl-2,6-dimethylpyridine derivatives was achieved in good to excellent yields by reaction of anilines with 3,5-bis（3＇,5＇-dimethy1-1＇-pyrazolyl-carbony1）-2,6- dimethylpyridine, in which pyrazoles served as leaving groups. The structure...

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Bibliographic Details
Published in:Chinese journal of chemistry 2011-10, Vol.29 (10), p.2119-2123
Main Author: 汪霞云 朱逸雯 张敏 陆东亮 钱群 陈雅丽 曹卫国 宋力平 邓红梅
Format: Article
Language:English
Subjects:
amide
aromatic amine
heterocycles
synthesis
二甲基吡啶
光谱数据
吡唑
吡啶衍生物
甲基衍生物
简便合成
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Summary:An efficient and convenient method for synthesis of 3,5-bis-carbamoyl-2,6-dimethylpyridine derivatives was achieved in good to excellent yields by reaction of anilines with 3,5-bis（3＇,5＇-dimethy1-1＇-pyrazolyl-carbony1）-2,6- dimethylpyridine, in which pyrazoles served as leaving groups. The structures of products were confirmed by spectra data and microanalysis.
ISSN:1001-604X
1614-7065
DOI:10.1002/cjoc.201180367