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Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge
A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecypari...
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Published in: | Chinese journal of chemistry 2011-08, Vol.29 (8), p.1759-1763 |
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container_title | Chinese journal of chemistry |
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creator | 朱涛 毕文韬 卢敬昊 |
description | A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. It provided a fast, economic and effective method for assaying trace drugs from natural plants. |
doi_str_mv | 10.1002/cjoc.201180280 |
format | article |
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After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. 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After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. It provided a fast, economic and effective method for assaying trace drugs from natural plants.</description><subject>extraction</subject><subject>ionic liquids</subject><subject>monolithic</subject><subject>myricetin</subject><subject>quercetin</subject><subject>单片</subject><subject>场发射扫描电子显微镜</subject><subject>墨盒</subject><subject>杨梅</subject><subject>槲皮素</subject><subject>离子液体</subject><subject>红桧</subject><subject>选择性提取</subject><issn>1001-604X</issn><issn>1614-7065</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkM9P2zAUx6OJSZSOK-dMO6d7jhMnOW4ZdEApmgCxm-U4L627Nm5tR5AD_zuGVBW3nfzjfT7vPX2D4IzAhADE3-VKy0kMhOQQ5_ApGBFGkigDlh75OwCJGCR_j4MTa1eez7KYjYKX82dnhHRKt6Fo6_AXOjQb1Yr3H92Efzo0Ep0ayje9UcOrMXoTlkuxESj7rTDKhrpynRVh1YeXulUynKldp2obVcKiV3Wr18otfaEUxhlVL_BL8LkRa4un-3McPFyc35e_o9nt9LL8MYskzQlEsUxEmlSxrHLG0qoSpCE5RUYpsERSrJu0jrFIJamxqhsq8kwShMKvVkMiJR0H34a-W6N3HVrHV7ozrR_JScZYDgUU1FOTgZJGW2uw4VujNsL0nAB_i5i_RcwPEXuhGIQntcb-PzQvr27Lj240uMo6fD64wvzjLKNZyh_nU371876cz4trfuf5r_vllrpd7FS7ODi0IBCnGaWvcfqdbw</recordid><startdate>201108</startdate><enddate>201108</enddate><creator>朱涛 毕文韬 卢敬昊</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><general>Wiley Subscription Services, Inc</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>~WA</scope><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>201108</creationdate><title>Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge</title><author>朱涛 毕文韬 卢敬昊</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>extraction</topic><topic>ionic liquids</topic><topic>monolithic</topic><topic>myricetin</topic><topic>quercetin</topic><topic>单片</topic><topic>场发射扫描电子显微镜</topic><topic>墨盒</topic><topic>杨梅</topic><topic>槲皮素</topic><topic>离子液体</topic><topic>红桧</topic><topic>选择性提取</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>朱涛 毕文韬 卢敬昊</creatorcontrib><collection>维普_期刊</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>Istex</collection><collection>CrossRef</collection><jtitle>Chinese journal of chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>朱涛 毕文韬 卢敬昊</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge</atitle><jtitle>Chinese journal of chemistry</jtitle><addtitle>Chinese Journal of Chemistry</addtitle><date>2011-08</date><risdate>2011</risdate><volume>29</volume><issue>8</issue><spage>1759</spage><epage>1763</epage><pages>1759-1763</pages><issn>1001-604X</issn><eissn>1614-7065</eissn><abstract>A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. It provided a fast, economic and effective method for assaying trace drugs from natural plants.</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/cjoc.201180280</doi><tpages>5</tpages></addata></record> |
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subjects | extraction ionic liquids monolithic myricetin quercetin 单片 场发射扫描电子显微镜 墨盒 杨梅 槲皮素 离子液体 红桧 选择性提取 |
title | Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge |
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