Loading…

Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge

A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecypari...

Full description

Saved in:
Bibliographic Details
Published in:Chinese journal of chemistry 2011-08, Vol.29 (8), p.1759-1763
Main Author: 朱涛 毕文韬 卢敬昊
Format: Article
Language:English
Subjects:
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3
cites cdi_FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3
container_end_page 1763
container_issue 8
container_start_page 1759
container_title Chinese journal of chemistry
container_volume 29
creator 朱涛 毕文韬 卢敬昊
description A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. It provided a fast, economic and effective method for assaying trace drugs from natural plants.
doi_str_mv 10.1002/cjoc.201180280
format article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_1766809093</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><cqvip_id>39102573</cqvip_id><sourcerecordid>3957985901</sourcerecordid><originalsourceid>FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3</originalsourceid><addsrcrecordid>eNqFkM9P2zAUx6OJSZSOK-dMO6d7jhMnOW4ZdEApmgCxm-U4L627Nm5tR5AD_zuGVBW3nfzjfT7vPX2D4IzAhADE3-VKy0kMhOQQ5_ApGBFGkigDlh75OwCJGCR_j4MTa1eez7KYjYKX82dnhHRKt6Fo6_AXOjQb1Yr3H92Efzo0Ep0ayje9UcOrMXoTlkuxESj7rTDKhrpynRVh1YeXulUynKldp2obVcKiV3Wr18otfaEUxhlVL_BL8LkRa4un-3McPFyc35e_o9nt9LL8MYskzQlEsUxEmlSxrHLG0qoSpCE5RUYpsERSrJu0jrFIJamxqhsq8kwShMKvVkMiJR0H34a-W6N3HVrHV7ozrR_JScZYDgUU1FOTgZJGW2uw4VujNsL0nAB_i5i_RcwPEXuhGIQntcb-PzQvr27Lj240uMo6fD64wvzjLKNZyh_nU371876cz4trfuf5r_vllrpd7FS7ODi0IBCnGaWvcfqdbw</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1766809093</pqid></control><display><type>article</type><title>Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge</title><source>Wiley-Blackwell Read &amp; Publish Collection</source><creator>朱涛 毕文韬 卢敬昊</creator><creatorcontrib>朱涛 毕文韬 卢敬昊</creatorcontrib><description>A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. It provided a fast, economic and effective method for assaying trace drugs from natural plants.</description><identifier>ISSN: 1001-604X</identifier><identifier>EISSN: 1614-7065</identifier><identifier>DOI: 10.1002/cjoc.201180280</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>extraction ; ionic liquids ; monolithic ; myricetin ; quercetin ; 单片 ; 场发射扫描电子显微镜 ; 墨盒 ; 杨梅 ; 槲皮素 ; 离子液体 ; 红桧 ; 选择性提取</subject><ispartof>Chinese journal of chemistry, 2011-08, Vol.29 (8), p.1759-1763</ispartof><rights>Copyright © 2011 SIOC, CAS, Shanghai &amp; WILEY‐VCH Verlag GmbH &amp; Co. KGaA, Weinheim</rights><rights>Copyright © 2011 SIOC, CAS, Shanghai &amp; WILEY-VCH Verlag GmbH &amp; Co. KGaA, Weinheim</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3</citedby><cites>FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/84126X/84126X.jpg</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>朱涛 毕文韬 卢敬昊</creatorcontrib><title>Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge</title><title>Chinese journal of chemistry</title><addtitle>Chinese Journal of Chemistry</addtitle><description>A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. It provided a fast, economic and effective method for assaying trace drugs from natural plants.</description><subject>extraction</subject><subject>ionic liquids</subject><subject>monolithic</subject><subject>myricetin</subject><subject>quercetin</subject><subject>单片</subject><subject>场发射扫描电子显微镜</subject><subject>墨盒</subject><subject>杨梅</subject><subject>槲皮素</subject><subject>离子液体</subject><subject>红桧</subject><subject>选择性提取</subject><issn>1001-604X</issn><issn>1614-7065</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkM9P2zAUx6OJSZSOK-dMO6d7jhMnOW4ZdEApmgCxm-U4L627Nm5tR5AD_zuGVBW3nfzjfT7vPX2D4IzAhADE3-VKy0kMhOQQ5_ApGBFGkigDlh75OwCJGCR_j4MTa1eez7KYjYKX82dnhHRKt6Fo6_AXOjQb1Yr3H92Efzo0Ep0ayje9UcOrMXoTlkuxESj7rTDKhrpynRVh1YeXulUynKldp2obVcKiV3Wr18otfaEUxhlVL_BL8LkRa4un-3McPFyc35e_o9nt9LL8MYskzQlEsUxEmlSxrHLG0qoSpCE5RUYpsERSrJu0jrFIJamxqhsq8kwShMKvVkMiJR0H34a-W6N3HVrHV7ozrR_JScZYDgUU1FOTgZJGW2uw4VujNsL0nAB_i5i_RcwPEXuhGIQntcb-PzQvr27Lj240uMo6fD64wvzjLKNZyh_nU371876cz4trfuf5r_vllrpd7FS7ODi0IBCnGaWvcfqdbw</recordid><startdate>201108</startdate><enddate>201108</enddate><creator>朱涛 毕文韬 卢敬昊</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><general>Wiley Subscription Services, Inc</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>~WA</scope><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>201108</creationdate><title>Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge</title><author>朱涛 毕文韬 卢敬昊</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>extraction</topic><topic>ionic liquids</topic><topic>monolithic</topic><topic>myricetin</topic><topic>quercetin</topic><topic>单片</topic><topic>场发射扫描电子显微镜</topic><topic>墨盒</topic><topic>杨梅</topic><topic>槲皮素</topic><topic>离子液体</topic><topic>红桧</topic><topic>选择性提取</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>朱涛 毕文韬 卢敬昊</creatorcontrib><collection>维普_期刊</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>Istex</collection><collection>CrossRef</collection><jtitle>Chinese journal of chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>朱涛 毕文韬 卢敬昊</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge</atitle><jtitle>Chinese journal of chemistry</jtitle><addtitle>Chinese Journal of Chemistry</addtitle><date>2011-08</date><risdate>2011</risdate><volume>29</volume><issue>8</issue><spage>1759</spage><epage>1763</epage><pages>1759-1763</pages><issn>1001-604X</issn><eissn>1614-7065</eissn><abstract>A short ionic liquids (ILs)-based monolithic cartridge was prepared and used as the selective extraction sorbent. After the material was evaluated by field emission-scanning electron microscopy (FE-SEM), a new approach for the extraction and determination of quercetin and myricetin from Chamaecyparis obtusa (C. obtusa) by using ILs-based, monolithic cartridge system was developed. Chromatographic analysis was conducted on a C18 column with UV detection at 372 nm, an eluting solution consisting of acetonitrile-water (25/75, V/V) as the mobile phase, and a flow rate of 0.7 mLomin 1. A good linear relationship was demonstrated when the concentrations of quercetin and myricetin were in the range of 0.5--100.0 ggomL-1. The recoveries ranged from 101.6% to 104.6% and the inter- and intra-day relative standard deviations (RSD) were less than 5.0%. This method effectively removed the impurities and avoided tedious pretreatment. It provided a fast, economic and effective method for assaying trace drugs from natural plants.</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/cjoc.201180280</doi><tpages>5</tpages></addata></record>
fulltext fulltext
identifier ISSN: 1001-604X
ispartof Chinese journal of chemistry, 2011-08, Vol.29 (8), p.1759-1763
issn 1001-604X
1614-7065
language eng
recordid cdi_proquest_journals_1766809093
source Wiley-Blackwell Read & Publish Collection
subjects extraction
ionic liquids
monolithic
myricetin
quercetin
单片
场发射扫描电子显微镜
墨盒
杨梅
槲皮素
离子液体
红桧
选择性提取
title Extraction and Determination of Quercetin and Myricetin from Chamaecyparis obtusa by Ionic Liquids-based Monolithic Cartridge
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-12T15%3A10%3A44IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Extraction%20and%20Determination%20of%20Quercetin%20and%20Myricetin%20from%20Chamaecyparis%20obtusa%20by%20Ionic%20Liquids-based%20Monolithic%20Cartridge&rft.jtitle=Chinese%20journal%20of%20chemistry&rft.au=%E6%9C%B1%E6%B6%9B%20%E6%AF%95%E6%96%87%E9%9F%AC%20%E5%8D%A2%E6%95%AC%E6%98%8A&rft.date=2011-08&rft.volume=29&rft.issue=8&rft.spage=1759&rft.epage=1763&rft.pages=1759-1763&rft.issn=1001-604X&rft.eissn=1614-7065&rft_id=info:doi/10.1002/cjoc.201180280&rft_dat=%3Cproquest_cross%3E3957985901%3C/proquest_cross%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c3810-2c4a54b2cb8665bba1f183e633064c3edf5d2e95c1debdf3a87c1e09aecd04cc3%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=1766809093&rft_id=info:pmid/&rft_cqvip_id=39102573&rfr_iscdi=true