Sequential Prins/Pinacol Strategy for the Stereoselective Synthesis of Spiro-[beta]-tetralones

A one-pot strategy has been developed for the stereoselective synthesis of 3',4,4',5-tetrahydro-2H,2'H-spiro(furan-3,1'-naphthalen)-2'-one scaffolds with excellent selectivity by using trimethylsilyl triflate (10mol%) in dichloromethane under mild conditions. The Prins/pinac...

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Published in:Asian journal of organic chemistry 2016-03, Vol.5 (3), p.411
Main Authors: Reddy, B V Subba, Raju, N Prudhvi, Reddy, B Jagan Mohan, Sridhar, B
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Organic chemistry
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Raju, N Prudhvi
Reddy, B Jagan Mohan
Sridhar, B
description A one-pot strategy has been developed for the stereoselective synthesis of 3',4,4',5-tetrahydro-2H,2'H-spiro(furan-3,1'-naphthalen)-2'-one scaffolds with excellent selectivity by using trimethylsilyl triflate (10mol%) in dichloromethane under mild conditions. The Prins/pinacol strategy has been used to produce biologically relevant spiro-[beta]-tetralone derivatives.
doi_str_mv 10.1002/ajoc.201500445
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title Sequential Prins/Pinacol Strategy for the Stereoselective Synthesis of Spiro-[beta]-tetralones
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