Crystal structure of phenylhydrazine with diacetyl substituted ketol of the cyclohexane series

The reaction of 2,4-diacetyl-5-hydroxy-5-methyl-3-phenylcyclohexanone-1 with phenylhydrazine is conducted, and the crystal structures of its products, 1-(6-hydroxy-3,6-dimethyl)-2,4-diphenyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)ethane-1-one and 1-(2-hydroxy-2-methyl-6-phenyl-4-(2-phenylhydrazono)-5-(1...

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Bibliographic Details
Published in:Journal of structural chemistry 2016-07, Vol.57 (4), p.764-770
Main Authors: Maharramov, A. M., Ismiyev, A. I., Allahverdiyev, M. A., Maleev, A. V., Potekhin, K. A.
Format: Article
Language:English
Subjects:
Atomic
Atomic/Molecular Structure and Spectra
Chemistry
Chemistry and Materials Science
Crystal structure
Cyclohexane
Ethane
Inorganic Chemistry
Molecular
Optical and Plasma Physics
Physical Chemistry
Single crystals
Solid State Physics
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Summary:The reaction of 2,4-diacetyl-5-hydroxy-5-methyl-3-phenylcyclohexanone-1 with phenylhydrazine is conducted, and the crystal structures of its products, 1-(6-hydroxy-3,6-dimethyl)-2,4-diphenyl-4,5,6,7-tetrahydro-2H-indazol-5-yl)ethane-1-one and 1-(2-hydroxy-2-methyl-6-phenyl-4-(2-phenylhydrazono)-5-(1-(2-henylhydrazono)ethyl)cyclohexyl)ethane-1-one, are determined by single crystal XRD.
ISSN:0022-4766
1573-8779
DOI:10.1134/S002247661604020X