Certification of the Melt Flow Index of a Polymeric Reference Material Based on a Proficiency Testing Scheme

• Published in: MĀPAN : journal of Metrology Society of India 2017-06, Vol.32 (2), p.149-154
• Main Authors: de Medeiros Albano, Filipe, Pizzolato, Morgana, Rodrigues, Thais Medeiros
• Format: Article
• Language: English
• Subjects: Borders; Case Report; Certification; ISO standards; Mathematical and Computational Physics; Mathematical Methods in Physics; Measurement Science and Instrumentation; Melt flow index; Numerical and Computational Physics; Physics; Physics and Astronomy; Polymers; Quality standards; Reference materials; Simulation; Theoretical; Time measurement; Uncertainty; Variance analysis
• ISSN: 0970-3950; 0974-9853
• DOI: 10.1007/s12647-017-0206-8

In order to be comparable across borders and over time, measurements need be traceable to appropriate and stated references. This paper discusses a proposal of a certification process of a Reference Material (RM) developed by an accredited Brazilian Proficiency Testing (PT) provider and a polymers industry. The RM was prepared for a PT scheme, based on ISO/IEC 17043, and also followed the production requirements of ISO Guide 34. PT Scheme data were evaluated based on ISO 13528 and the certification process followed the Annex B of ISO GUIDE 35. The proposal presented in this paper was based on a certification of the melt flow index of a polymer. The results indicate that certification process was fit for the plastic company purpose and that the use of ANOVA was adequate to establish Certified Reference Material uncertainty.