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Chemical stability of carbon-based inorganic materials for in situ x-ray investigations of ammonothermal crystal growth of nitrides
The chemical stability of diamond, silicon carbide, vitreous carbon, and boron carbide in supercritical ammonia containing different mineralizers was investigated. The materials were found to show good corrosion resistance in the presence of selective or all tested mineralizers. Diamond was found to...
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| Published in: | Journal of crystal growth 2016-12, Vol.456, p.33-42 |
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| Main Authors: | , , , , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c406t-43d3d1892b526c5f50463a7edcf5ec76d7036718dc7d0d2462fff8597bac91173 |
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| cites | cdi_FETCH-LOGICAL-c406t-43d3d1892b526c5f50463a7edcf5ec76d7036718dc7d0d2462fff8597bac91173 |
| container_end_page | 42 |
| container_issue | |
| container_start_page | 33 |
| container_title | Journal of crystal growth |
| container_volume | 456 |
| creator | Schimmel, Saskia Künecke, Ulrike Meisel, Magnus Hertweck, Benjamin Steigerwald, Thomas G. Nebel, Christoph Alt, Nicolas S.A. Schlücker, Eberhard Wellmann, Peter |
| description | The chemical stability of diamond, silicon carbide, vitreous carbon, and boron carbide in supercritical ammonia containing different mineralizers was investigated. The materials were found to show good corrosion resistance in the presence of selective or all tested mineralizers.
Diamond was found to be virtually inert in both ammonoacidic and ammonobasic reaction media.
Silicon carbide showed good chemical stability in varying ammonothermal reaction media.
The chemical stability of vitreous carbon was found to depend on its manufacturing temperature.
Corrosion of boron carbide strongly depends on the mineralizer used as well as on applied mechanical stress.
Based on their chemical stability and mechanical properties, the applicability of the materials in the respective ammonothermal reaction media as construction materials is evaluated. Additionally, the applicability of the materials as a window material for both high energy in situ x-ray imaging and low energy in situ x-ray diffraction is discussed.
•Chemical stability of carbon-based inorganic materials is investigated.•Window materials for low energy in situ x-ray diffraction are identified.•Window materials are applicable under ammonothermal conditions. |
| doi_str_mv | 10.1016/j.jcrysgro.2016.08.067 |
| format | article |
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Diamond was found to be virtually inert in both ammonoacidic and ammonobasic reaction media.
Silicon carbide showed good chemical stability in varying ammonothermal reaction media.
The chemical stability of vitreous carbon was found to depend on its manufacturing temperature.
Corrosion of boron carbide strongly depends on the mineralizer used as well as on applied mechanical stress.
Based on their chemical stability and mechanical properties, the applicability of the materials in the respective ammonothermal reaction media as construction materials is evaluated. Additionally, the applicability of the materials as a window material for both high energy in situ x-ray imaging and low energy in situ x-ray diffraction is discussed.
•Chemical stability of carbon-based inorganic materials is investigated.•Window materials for low energy in situ x-ray diffraction are identified.•Window materials are applicable under ammonothermal conditions.</description><identifier>ISSN: 0022-0248</identifier><identifier>EISSN: 1873-5002</identifier><identifier>DOI: 10.1016/j.jcrysgro.2016.08.067</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>A1. Solubility ; A1. Solvents ; A1. X-ray diffraction ; A2. Ammonothermal crystal growth ; Ammonia ; B1. Inorganic compounds ; B1. Nitrides ; Boron carbide ; Carbon ; Construction materials ; Corrosion ; Corrosion resistance ; Corrosion tests ; Crystals ; Diamonds ; Inorganic materials ; Mechanical properties ; Nitrides ; Silicon carbide ; Stability ; X-ray diffraction</subject><ispartof>Journal of crystal growth, 2016-12, Vol.456, p.33-42</ispartof><rights>2016 Elsevier B.V.</rights><rights>Copyright Elsevier BV Dec 15, 2016</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c406t-43d3d1892b526c5f50463a7edcf5ec76d7036718dc7d0d2462fff8597bac91173</citedby><cites>FETCH-LOGICAL-c406t-43d3d1892b526c5f50463a7edcf5ec76d7036718dc7d0d2462fff8597bac91173</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,777,781,27906,27907</link.rule.ids></links><search><creatorcontrib>Schimmel, Saskia</creatorcontrib><creatorcontrib>Künecke, Ulrike</creatorcontrib><creatorcontrib>Meisel, Magnus</creatorcontrib><creatorcontrib>Hertweck, Benjamin</creatorcontrib><creatorcontrib>Steigerwald, Thomas G.</creatorcontrib><creatorcontrib>Nebel, Christoph</creatorcontrib><creatorcontrib>Alt, Nicolas S.A.</creatorcontrib><creatorcontrib>Schlücker, Eberhard</creatorcontrib><creatorcontrib>Wellmann, Peter</creatorcontrib><title>Chemical stability of carbon-based inorganic materials for in situ x-ray investigations of ammonothermal crystal growth of nitrides</title><title>Journal of crystal growth</title><description>The chemical stability of diamond, silicon carbide, vitreous carbon, and boron carbide in supercritical ammonia containing different mineralizers was investigated. The materials were found to show good corrosion resistance in the presence of selective or all tested mineralizers.
Diamond was found to be virtually inert in both ammonoacidic and ammonobasic reaction media.
Silicon carbide showed good chemical stability in varying ammonothermal reaction media.
The chemical stability of vitreous carbon was found to depend on its manufacturing temperature.
Corrosion of boron carbide strongly depends on the mineralizer used as well as on applied mechanical stress.
Based on their chemical stability and mechanical properties, the applicability of the materials in the respective ammonothermal reaction media as construction materials is evaluated. Additionally, the applicability of the materials as a window material for both high energy in situ x-ray imaging and low energy in situ x-ray diffraction is discussed.
•Chemical stability of carbon-based inorganic materials is investigated.•Window materials for low energy in situ x-ray diffraction are identified.•Window materials are applicable under ammonothermal conditions.</description><subject>A1. Solubility</subject><subject>A1. Solvents</subject><subject>A1. X-ray diffraction</subject><subject>A2. Ammonothermal crystal growth</subject><subject>Ammonia</subject><subject>B1. Inorganic compounds</subject><subject>B1. Nitrides</subject><subject>Boron carbide</subject><subject>Carbon</subject><subject>Construction materials</subject><subject>Corrosion</subject><subject>Corrosion resistance</subject><subject>Corrosion tests</subject><subject>Crystals</subject><subject>Diamonds</subject><subject>Inorganic materials</subject><subject>Mechanical properties</subject><subject>Nitrides</subject><subject>Silicon carbide</subject><subject>Stability</subject><subject>X-ray diffraction</subject><issn>0022-0248</issn><issn>1873-5002</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNqFkElPwzAQhS0EEmX5CygS5wQviZ3eQBWbVIkLnC3HS-uoiWHsFnrmj-OocObi0dhvvnl-CF0RXBFM-E1f9Rr2cQWhormvcFthLo7QjLSClQ3G9BjN8klLTOv2FJ3F2GOclQTP0PdibQev1aaISXV-49O-CK7QCrowlp2K1hR-DLBSo9fFoJIFrzaxcAHyfRF92hZfJah97nY2Jr9SyYcxThA1DGEMaW1hyPzJY8o1-_xM6-l99Am8sfECnbjMtJe_9Ry9Pdy_Lp7K5cvj8-JuWeoa81TWzDBD2jntGsp14xpcc6aENdo1VgtuBGZckNZoYbChNafOubaZi07pOSGCnaPrA_cdwsc2m5V92MKYV0oyZ4xmLONZxQ8qDSFGsE6-gx8U7CXBcgpc9vIvcDkFLnErc-B58PYwaPMfdt6CjNrbUVvjweokTfD_IX4AP5SQYw</recordid><startdate>20161215</startdate><enddate>20161215</enddate><creator>Schimmel, Saskia</creator><creator>Künecke, Ulrike</creator><creator>Meisel, Magnus</creator><creator>Hertweck, Benjamin</creator><creator>Steigerwald, Thomas G.</creator><creator>Nebel, Christoph</creator><creator>Alt, Nicolas S.A.</creator><creator>Schlücker, Eberhard</creator><creator>Wellmann, Peter</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20161215</creationdate><title>Chemical stability of carbon-based inorganic materials for in situ x-ray investigations of ammonothermal crystal growth of nitrides</title><author>Schimmel, Saskia ; Künecke, Ulrike ; Meisel, Magnus ; Hertweck, Benjamin ; Steigerwald, Thomas G. ; Nebel, Christoph ; Alt, Nicolas S.A. ; Schlücker, Eberhard ; Wellmann, Peter</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c406t-43d3d1892b526c5f50463a7edcf5ec76d7036718dc7d0d2462fff8597bac91173</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>A1. Solubility</topic><topic>A1. Solvents</topic><topic>A1. X-ray diffraction</topic><topic>A2. Ammonothermal crystal growth</topic><topic>Ammonia</topic><topic>B1. Inorganic compounds</topic><topic>B1. Nitrides</topic><topic>Boron carbide</topic><topic>Carbon</topic><topic>Construction materials</topic><topic>Corrosion</topic><topic>Corrosion resistance</topic><topic>Corrosion tests</topic><topic>Crystals</topic><topic>Diamonds</topic><topic>Inorganic materials</topic><topic>Mechanical properties</topic><topic>Nitrides</topic><topic>Silicon carbide</topic><topic>Stability</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Schimmel, Saskia</creatorcontrib><creatorcontrib>Künecke, Ulrike</creatorcontrib><creatorcontrib>Meisel, Magnus</creatorcontrib><creatorcontrib>Hertweck, Benjamin</creatorcontrib><creatorcontrib>Steigerwald, Thomas G.</creatorcontrib><creatorcontrib>Nebel, Christoph</creatorcontrib><creatorcontrib>Alt, Nicolas S.A.</creatorcontrib><creatorcontrib>Schlücker, Eberhard</creatorcontrib><creatorcontrib>Wellmann, Peter</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of crystal growth</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Schimmel, Saskia</au><au>Künecke, Ulrike</au><au>Meisel, Magnus</au><au>Hertweck, Benjamin</au><au>Steigerwald, Thomas G.</au><au>Nebel, Christoph</au><au>Alt, Nicolas S.A.</au><au>Schlücker, Eberhard</au><au>Wellmann, Peter</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Chemical stability of carbon-based inorganic materials for in situ x-ray investigations of ammonothermal crystal growth of nitrides</atitle><jtitle>Journal of crystal growth</jtitle><date>2016-12-15</date><risdate>2016</risdate><volume>456</volume><spage>33</spage><epage>42</epage><pages>33-42</pages><issn>0022-0248</issn><eissn>1873-5002</eissn><abstract>The chemical stability of diamond, silicon carbide, vitreous carbon, and boron carbide in supercritical ammonia containing different mineralizers was investigated. The materials were found to show good corrosion resistance in the presence of selective or all tested mineralizers.
Diamond was found to be virtually inert in both ammonoacidic and ammonobasic reaction media.
Silicon carbide showed good chemical stability in varying ammonothermal reaction media.
The chemical stability of vitreous carbon was found to depend on its manufacturing temperature.
Corrosion of boron carbide strongly depends on the mineralizer used as well as on applied mechanical stress.
Based on their chemical stability and mechanical properties, the applicability of the materials in the respective ammonothermal reaction media as construction materials is evaluated. Additionally, the applicability of the materials as a window material for both high energy in situ x-ray imaging and low energy in situ x-ray diffraction is discussed.
•Chemical stability of carbon-based inorganic materials is investigated.•Window materials for low energy in situ x-ray diffraction are identified.•Window materials are applicable under ammonothermal conditions.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jcrysgro.2016.08.067</doi><tpages>10</tpages></addata></record> |
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| identifier | ISSN: 0022-0248 |
| ispartof | Journal of crystal growth, 2016-12, Vol.456, p.33-42 |
| issn | 0022-0248 1873-5002 |
| language | eng |
| recordid | cdi_proquest_journals_1933252636 |
| source | Elsevier:Jisc Collections:Elsevier Read and Publish Agreement 2022-2024:Freedom Collection (Reading list) |
| subjects | A1. Solubility A1. Solvents A1. X-ray diffraction A2. Ammonothermal crystal growth Ammonia B1. Inorganic compounds B1. Nitrides Boron carbide Carbon Construction materials Corrosion Corrosion resistance Corrosion tests Crystals Diamonds Inorganic materials Mechanical properties Nitrides Silicon carbide Stability X-ray diffraction |
| title | Chemical stability of carbon-based inorganic materials for in situ x-ray investigations of ammonothermal crystal growth of nitrides |
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