Tuning of mechanical and structural properties of 20 MC 5 steel using N ion implantation and subsequent annealing

• Published in: Journal of alloys and compounds 2017-07, Vol.710, p.253-259
• Main Authors: Singh, Omveer, Malik, Hitendra K., Dahiya, Raj P., Kulriya, P.K.
• Format: Article
• Language: English
• Subjects: 20 MC 5 steel; Annealing; Atomic force microscopy; Atomic structure; Crankshafts; Fluence; Gears; Hardness; Hardness testing; Ion implantation; Machinery and equipment; Mechanical properties; Nitrogen; Phase transitions; Steel; Surface roughness
• ISSN: 0925-8388; 1873-4669
• DOI: 10.1016/j.jallcom.2017.03.097

In the present work, effect of 50 keV nitrogen ion implantation on the structure and mechanical properties of as-implanted and annealed 20 MC 5 steel samples is investigated. XRD measurements confirmed the formation of α−FeN phase. The crystallite size and stress of the nitride samples is found to increase with the ion fluence. The calculated value of crystallite size and stress is ∼29.21 nm and ∼9.826 × 108 Pa, respectively, for 1 × 1016 ions/cm2 implanted sample. An increase in crystallite size (∼31.26 nm) and phase transformation from FeN phase to Fe2-3N and Fe4N phase is observed on annealing at 500 °C for 2 h. Atomic force microscopy results show that surface roughness and particle size are increasing with ion fluence. Mechanical properties studied using Micro-Vicker hardness tester showed that hardness of the annealed sample increases initially with ions fluences (∼8.4 GPa at 1 × 1015 ions/cm2) and then it starts decreasing to ∼4.66 GPa when sample is exposed to an ion fluence of 1 × 1016, due to limited solubility of nitrogen in steel. Finally, we have performed simulations using TRIM software to investigate the impurity profile in the samples under the influence of 50 keV ions. Our results show that the ion implantation technique is very good tool for controlled modification of mechanical properties of 20 MC 5 steel, and it can be used in various applications such as crankshafts, gears, engines and machinery parts. •To study the influence of N on various physical properties of 20 MC 5 steel samples.•N wt% and microhardness of annealed samples increases with ions fluence.•Phase transformation from FeN phase to Fe2-3N & Fe4N phase occurs on annealing.•Hardness of annealed samples increases initially and decreases for higher fluences.