Microstructure evolution and mechanical properties of a high strength Mg-11.7Gd-4.9Y-0.3Zr (wt%) alloy prepared by pre-deformation annealing, hot extrusion and ageing

• Published in: Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2017-08, Vol.703, p.348-358
• Main Authors: Yu, Zijian, Xu, Chao, Meng, Jian, Kamado, Shigeharu
• Format: Article
• Language: English
• Subjects: Aging (metallurgy); Annealing; Asymmetry; Compressive strength; Continuous extrusion; Deformation effects; Dynamic recrystallization; Elongation; Evolution; Extrusion; Grain refinement; High strength; Hot extrusion; Magnesium; Magnesium alloy; Mechanical properties; Mechanical property; Microstructure; Pre-deformation annealing; Rare earth; Rare earth elements; Recrystallization behavior; Texture; Yield strength
• ISSN: 0921-5093; 1873-4936
• DOI: 10.1016/j.msea.2017.06.096

A high strength Mg-11.7Gd-4.9Y-0.3Zr (wt%) alloy with a weak tension-compression yield asymmetry has been successfully developed by pre-deformation annealing, hot extrusion and ageing. The effects of pre-deformation annealing on the microstructure evolution and mechanical properties are studied. The results reveal that pre-deformation annealing generates a large number of Mg5RE (RE: rare earth) phase particles and raises the fraction of dynamic recrystallization (DRX). The preformed Mg5RE particles not only enhance the DRX by particle simulated nucleation (PSN), but also facilitate the continuous DRX (C-DRX) by promoting the grain subdivision during hot extrusion. Without pre-deformation annealing, the as-extruded alloy exhibits a high tensile yield strength (TYS) of 376 ± 9.6MPa but a low elongation to failure (EL) of 4.3 ± 0.1% due to the bimodal microstructure consisting of coarse un-DRXed grains with strong basal texture and fine DRXed grains with weak basal texture. After T5 treatment, the TYS further increases to 500 ± 5.5MPa, whereas the EL reduces to 2.7 ± 0.4%. An excellent balance of strength and ductility (TYS of 343 ± 0.2MPa and EL of 9.3 ± 0.9%) can be realized by pre-deformation annealing for 1h due to the raised fraction of DRX and the weakened basal texture. T5 treatment further increases the TYS to 446 ± 3.8MPa but reduces the EL to 3.0 ± 0.2%. The studied alloy exhibits good compressive performance, resulting in a weak tension-compression yield asymmetry. The grain refinement, Mg5RE and β′ phases, and solute-segregated SFs contribute to the alloy strengthening. •A Mg alloy with a YS of 500 ± 5.5MPa and an elongation of 2.7 ± 0.4% was produced.•The pre-deformation annealing affects the post-extrusion microstructures.•The balanced strength and ductility is achieved by pre-deformation annealing for 1h.•The preformed Mg5RE particles lead to DRX by PSN and enhance C-DRX.