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Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates
The microwave-assisted reaction of (TBA) 4 [β-Mo 8 O 24 ] and (TBA) 3 [H 3 V 10 O 28 ] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA) 2 [V 3 Mo 3 O 16 (O 3 –R)] (R: C 5 H 8 OH – 1 ; R: C 4 H 6 NH 2 – 3 ). Post-synthetic esterification of 1 yi...
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Published in: | New journal of chemistry 2018, Vol.42 (1), p.25-28 |
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container_title | New journal of chemistry |
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creator | Karoui, H. Ritchie, C. |
description | The microwave-assisted reaction of (TBA)
4
[β-Mo
8
O
24
] and (TBA)
3
[H
3
V
10
O
28
] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)
2
[V
3
Mo
3
O
16
(O
3
–R)] (R: C
5
H
8
OH –
1
; R: C
4
H
6
NH
2
–
3
). Post-synthetic esterification of
1
yields the acylated derivative
2
, with all compounds being characterized in the solid and solution state. |
doi_str_mv | 10.1039/C7NJ02820B |
format | article |
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4
[β-Mo
8
O
24
] and (TBA)
3
[H
3
V
10
O
28
] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)
2
[V
3
Mo
3
O
16
(O
3
–R)] (R: C
5
H
8
OH –
1
; R: C
4
H
6
NH
2
–
3
). Post-synthetic esterification of
1
yields the acylated derivative
2
, with all compounds being characterized in the solid and solution state.</description><identifier>ISSN: 1144-0546</identifier><identifier>EISSN: 1369-9261</identifier><identifier>DOI: 10.1039/C7NJ02820B</identifier><language>eng</language><publisher>Cambridge: Royal Society of Chemistry</publisher><subject>Chemical synthesis ; Esterification</subject><ispartof>New journal of chemistry, 2018, Vol.42 (1), p.25-28</ispartof><rights>Copyright Royal Society of Chemistry 2018</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c295t-baa2abc27c9f47fafce704f6edbdb71d6d7df796ab0a5643f26eacf98acf04c73</citedby><cites>FETCH-LOGICAL-c295t-baa2abc27c9f47fafce704f6edbdb71d6d7df796ab0a5643f26eacf98acf04c73</cites><orcidid>0000-0002-1640-6406</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,778,782,4012,27906,27907,27908</link.rule.ids></links><search><creatorcontrib>Karoui, H.</creatorcontrib><creatorcontrib>Ritchie, C.</creatorcontrib><title>Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates</title><title>New journal of chemistry</title><description>The microwave-assisted reaction of (TBA)
4
[β-Mo
8
O
24
] and (TBA)
3
[H
3
V
10
O
28
] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)
2
[V
3
Mo
3
O
16
(O
3
–R)] (R: C
5
H
8
OH –
1
; R: C
4
H
6
NH
2
–
3
). Post-synthetic esterification of
1
yields the acylated derivative
2
, with all compounds being characterized in the solid and solution state.</description><subject>Chemical synthesis</subject><subject>Esterification</subject><issn>1144-0546</issn><issn>1369-9261</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNpFkEtPwzAQhC0EEqVw4RdE4oZkWDuuXR-h4qnyOMA52vhBU6VxsZNC-PWkKhKX3R3p02pmCDllcMEg15cz9fwIfMrheo-MWC411Vyy_eFmQlCYCHlIjlJaAjCmJBuR16fKxPCFG0cxpSq1zmapb9qFG0QWfBbiBzaVwbruM981pq1Cg3X1M3AL9410Feq-tGGDDVpsXTomBx7r5E7-9pi83968ze7p_OXuYXY1p4brSUtLRI6l4cpoL5RHb5wC4aWzpS0Vs9Iq65WWWAJOpMg9lw6N19NhgDAqH5Oz3d91DJ-dS22xDF0crKWCA4Op4jlsqfMdNYRMKTpfrGO1wtgXDIptY8V_Y_kvNblhFg</recordid><startdate>2018</startdate><enddate>2018</enddate><creator>Karoui, H.</creator><creator>Ritchie, C.</creator><general>Royal Society of Chemistry</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>H9R</scope><scope>JG9</scope><scope>KA0</scope><orcidid>https://orcid.org/0000-0002-1640-6406</orcidid></search><sort><creationdate>2018</creationdate><title>Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates</title><author>Karoui, H. ; Ritchie, C.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c295t-baa2abc27c9f47fafce704f6edbdb71d6d7df796ab0a5643f26eacf98acf04c73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Chemical synthesis</topic><topic>Esterification</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Karoui, H.</creatorcontrib><creatorcontrib>Ritchie, C.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Illustrata: Natural Sciences</collection><collection>Materials Research Database</collection><collection>ProQuest Illustrata: Technology Collection</collection><jtitle>New journal of chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Karoui, H.</au><au>Ritchie, C.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates</atitle><jtitle>New journal of chemistry</jtitle><date>2018</date><risdate>2018</risdate><volume>42</volume><issue>1</issue><spage>25</spage><epage>28</epage><pages>25-28</pages><issn>1144-0546</issn><eissn>1369-9261</eissn><abstract>The microwave-assisted reaction of (TBA)
4
[β-Mo
8
O
24
] and (TBA)
3
[H
3
V
10
O
28
] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)
2
[V
3
Mo
3
O
16
(O
3
–R)] (R: C
5
H
8
OH –
1
; R: C
4
H
6
NH
2
–
3
). Post-synthetic esterification of
1
yields the acylated derivative
2
, with all compounds being characterized in the solid and solution state.</abstract><cop>Cambridge</cop><pub>Royal Society of Chemistry</pub><doi>10.1039/C7NJ02820B</doi><tpages>4</tpages><orcidid>https://orcid.org/0000-0002-1640-6406</orcidid><oa>free_for_read</oa></addata></record> |
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issn | 1144-0546 1369-9261 |
language | eng |
recordid | cdi_proquest_journals_2010872307 |
source | Royal Society of Chemistry Journals |
subjects | Chemical synthesis Esterification |
title | Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates |
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