Single‐crystal neutron diffraction in diamond anvil cells with hot neutrons

It is demonstrated that it is possible to perform single‐crystal measurements in diamond anvil cells (DACs) with a monochromatic beam at modern hot neutron sources that offer the benefit of short neutron wavelengths with high fluxes. A piston–cylinder DAC with conical Boehler–Almax diamonds that all...

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Published in:Journal of applied crystallography 2018-04, Vol.51 (2), p.351-356
Main Authors: Grzechnik, Andrzej, Meven, Martin, Friese, Karen
Format: Article
Language:English
Subjects:
Cylinders
Diamond anvil cells
Diamonds
Diffraction
Fluxes
high pressure
hot neutrons
Neutron diffraction
Neutron sources
Neutrons
single‐crystal diffraction
Wavelengths
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cited_by cdi_FETCH-LOGICAL-c3230-7ae2cf9117ef99d68b4900e0252b49623eeaea68842bf10eef5595e734f162113
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description It is demonstrated that it is possible to perform single‐crystal measurements in diamond anvil cells (DACs) with a monochromatic beam at modern hot neutron sources that offer the benefit of short neutron wavelengths with high fluxes. A piston–cylinder DAC with conical Boehler–Almax diamonds that allows for a wide accessibility of the reciprocal space has been developed. The diffraction data collected in this cell using hot neutrons are of very good quality and can be used for a full and reliable structure refinement. It is shown that it is possible to perform single‐crystal measurements in diamond anvil cells with a monochromatic beam at modern hot neutron sources. The data are of very good quality and can be used for a full and reliable structure refinement.
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source Wiley-Blackwell Read & Publish Collection
subjects Cylinders
Diamond anvil cells
Diamonds
Diffraction
Fluxes
high pressure
hot neutrons
Neutron diffraction
Neutron sources
Neutrons
single‐crystal diffraction
Wavelengths
title Single‐crystal neutron diffraction in diamond anvil cells with hot neutrons
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