The critical parameters in in-situ MgB2 wires and tapes with ex-situ MgB2 barrier after hot isostatic pressure, cold drawing, cold rolling and doping

• Published in: Journal of applied physics 2015-05, Vol.117 (17)
• Main Authors: Gajda, D., Morawski, A., Zaleski, A. J., Häßler, W., Nenkov, K., Rindfleisch, M. A., Żuchowska, E., Gajda, G., Czujko, T., Cetner, T, Hossain, M. S. A.
• Format: Article
• Language: English
• Subjects: Applied physics; Barriers; Borides; Cold; Cold drawing; Cold isostatic pressing; Cold pressing; Cold rolling; Critical current density; Critical temperature; Doping; Isostatic pressure; Magnesium compounds; Magnetic fields; Pinning; Transport
• ISSN: 0021-8979; 1089-7550
• DOI: 10.1063/1.4919364

MgB2 precursor wires were prepared using powder in tube technique by Institute of High Pressure PAS in Warsaw. All samples were annealed under isostatic pressure generated by liquid Argon in the range from 0.3 GPa to 1 GPa. In this paper, we show the effects of different processing routes, namely, cold drawing (CD), cold rolling (CR), hot isostatic pressure (HIP) and doping on critical current density (Jc), pinning force (Fp), irreversible magnetic-field (Birr), critical temperature (Tc), n value, and dominant pinning mechanism in MgB2/Fe wires with ex situ MgB2 barrier. The results show that medium pressures (∼0.35 GPa) lead to high Jc in low and medium magnetic fields (0 T – 9 T). On the other hand, higher pressures (∼1 GPa) lead to enhanced Jc in high magnetic fields (above 9 T). Transport measurements show that CD, CR, and HIP have small effects on Birr and Tc, but CD, CR, HIP, and doping enhance Jc and Fp in in situ MgB2 wires with ex situ MgB2 barrier. Transport measurements on in situ undoped MgB2 wire with ex situ MgB2 barrier yield a Jc of about 100 A/mm2 at 4.2 K in 6 T, at 10 K in 4 T and at 20 K in 2 T. The results also show that cold drawing causes increase of n value.