Joint utilization of double-pulse laser-induced breakdown spectroscopy and X-ray computed tomography for volumetric information of geological samples

The purpose of this study is to present a novel algorithm to combine high-resolution X-ray Computed Tomography (HRXCT) and Double-Pulse Laser-Induced Breakdown Spectroscopy (DP LIBS) for geological samples' analysis. The ability to reveal the elemental composition of the internal structure is d...

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Bibliographic Details
Published in:Journal of analytical atomic spectrometry 2018-11, Vol.33 (11), p.1993-1999
Main Authors: Prochazka, D, Zikmund, T, Po ízka, P, B ínek, A, Klus, J, Šalplachta, J, Kynický, J, Novotný, J, Kaiser, J
Format: Article
Language:English
Subjects:
Computation
Computed tomography
Copper
Geology
Laser induced breakdown spectroscopy
Nickel
Spectrum analysis
X ray spectra
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Summary:The purpose of this study is to present a novel algorithm to combine high-resolution X-ray Computed Tomography (HRXCT) and Double-Pulse Laser-Induced Breakdown Spectroscopy (DP LIBS) for geological samples' analysis. The ability to reveal the elemental composition of the internal structure is demonstrated on a rare geological sample from a unique Talnakh PGE-Cu-Ni sulfide deposit. The main point of the suggested approach is to assign the DP LIBS elemental maps to the different densities of the HRXCT data. This assignment is based on the coordinates of the HRXCT data (top-cross section) and DP LIBS elemental maps of the surface. The resolution and orientation of these two images are aligned in order to enable a comparison. Moreover, the volumetric information about individual materials within the sample was estimated. Joint utilization of high-resolution X-ray computed tomography and laser-induced breakdown spectroscopy advanced 3D elemental imaging.
ISSN:0267-9477
1364-5544
DOI:10.1039/c8ja00232k