Using spherical indentation to measure the strength of copper-chromium-zirconium

• Published in: Journal of nuclear materials 2018-12, Vol.511, p.610-616
• Main Authors: Cackett, Alexandra J., Lim, Joven J.H., Klupś, Przemysław, Bushby, Andy J., Hardie, Christopher D.
• Format: Article
• Language: English
• Subjects: Alloys; Balances (scales); Chemical compounds; Chemical precipitation; Chromium; CuCrZr alloy; Deformation; Deformation mechanisms; Dislocation; Dislocations; Heat treatment; Irradiation; ISE; Mechanical analysis; Mechanical properties; Nanoindentation; Nuclear power plants; Plastic deformation; Plasticity; Radiation; Radioactive materials; Size effects; Spherical indentation; Strain; Stress-strain curves; Stress-strain relationships; Yield strength; Zirconium
• ISSN: 0022-3115; 1873-4820
• DOI: 10.1016/j.jnucmat.2018.04.012

Precipitation hardened CuCrZr will be used in heat-sink components in the ITER tokomak and is a primary candidate for EU DEMO. The measurement of mechanical properties of irradiated CuCrZr using conventional, standardised techniques is difficult due to the challenges involved in working with radioactive material and the relatively large specimen size required. Spherical nano-indentation offers a technique to measure stress-strain properties from far smaller volumes than conventional tests. In this work, CuCrZr has been heat-treated at different temperatures to vary the Cr precipitate size and spacing. Spherical nano-indentation using multiple tip radii was then used to produce stress-strain curves for all samples, from which values of initial flow stress were calculated. It was found that there was a strong indentation size effect (ISE) in the stress required to initiate plasticity, however at higher indentation strains the flow stress became constant for tip radii, R, ≥8 μm. This suggests that at the initiation of plastic deformation the ISE is dominated by dislocation source activation but in later stages the interaction with microstructural material length-scales dominate the measured mechanical strength. The mechanical response of these small-scale tests is governed by multiple mechanisms, which convolute interpretation of data and must be considered when measuring the effects of irradiation on the mechanical properties. •The hardness of CuCrZr was measured using spherical nano-indentation.•A strong indentation size effect was seen at low indentation strains.•The indentation size effect was suppressed at higher strains.