Reaction of sodium 4-acetyl-1-phenyl-1H-1,2,3-triazol-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide

The present work describes a method for the synthesis a new N-1,2,3-triazol-1-yl-1,2,3-thiadiazol-4-carboxamide via condensation of open-chain form of 4-acetyl-1,2,3-triazolium-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide, followed by formation new 1,2,3-triazole cycle. The structure o...

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Bibliographic Details
Main Authors: Tokareva, M. A., Obydennov, K. L., Slepukhin, P. A., Vysokova, O. A., Glukhareva, T. V.
Format: Conference Proceeding
Language:English
Subjects:
Mass spectrometry
NMR
Nuclear magnetic resonance
X-ray diffraction
Online Access:Get full text
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Summary:The present work describes a method for the synthesis a new N-1,2,3-triazol-1-yl-1,2,3-thiadiazol-4-carboxamide via condensation of open-chain form of 4-acetyl-1,2,3-triazolium-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide, followed by formation new 1,2,3-triazole cycle. The structure of synthesized compound was characterized by spectroscopic methods such as 1H NMR, 13C NMR, IR, mass spectrometry and X-ray diffraction.
ISSN:0094-243X
1551-7616
DOI:10.1063/1.5087392