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Universal Research Cryogenic Unit for Xenon Production
Xenon is a cryogenic product that is currently in short supply. Requirements for its purity are increasing. Its consumption in microelectronics, medicine, and space technology and for high-energy particle physics research is rising. The permissible impurity contents in Xe for various applications we...
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| Published in: | Chemical and petroleum engineering 2019-03, Vol.54 (11-12), p.806-814 |
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| Main Authors: | , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c429t-ce241672e1c34f93a9cb0e39cea826b6903da2ccc7f77181744c9d294f5e1fa23 |
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| cites | cdi_FETCH-LOGICAL-c429t-ce241672e1c34f93a9cb0e39cea826b6903da2ccc7f77181744c9d294f5e1fa23 |
| container_end_page | 814 |
| container_issue | 11-12 |
| container_start_page | 806 |
| container_title | Chemical and petroleum engineering |
| container_volume | 54 |
| creator | Bondarenko, V. L. Kupriyanov, M. Yu Ustyugova, T. G. Verkhovnyi, A. I. Stefanovskii, A. N. |
| description | Xenon is a cryogenic product that is currently in short supply. Requirements for its purity are increasing. Its consumption in microelectronics, medicine, and space technology and for high-energy particle physics research is rising. The permissible impurity contents in Xe for various applications were analyzed. A universal research cryogenic unit for Xe production of throughput up to 10 Nm
3
/h of feedstock mixture was designed. A scheme with separation by rectification and preliminary catalytic and adsorptive purification of the feedstock was chosen. The unit was built in blocks so that processing schemes for Xe production from various mixtures, e.g., Kr–Xe, Xe–N
2
, Xe–O
2
, could be studied. Trace impurities in Xe were analyzed by gas chromatographs with thermal conductivity (TCD), He-ionization (HID), and flame-ionization detectors (FID). Water vapor in the analyzed gases was measured using laseroptical and coulometric hygrometers. The first runs showed that the unit could produce Xe of purity up to 99.9999 %. Experimental data for rectification of Xe to a purity of 99.999 % are presented. Xe could be purified experimentally from traces of CF
4
, C
2
F
6
, SF
6
, hydrocarbons, CO
2
, and H
2
to 0.05; O
2
and N
2
, 0.1; Kr, 0.01; and water vapor, 0.2 ppm. |
| doi_str_mv | 10.1007/s10556-019-00554-4 |
| format | article |
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3
/h of feedstock mixture was designed. A scheme with separation by rectification and preliminary catalytic and adsorptive purification of the feedstock was chosen. The unit was built in blocks so that processing schemes for Xe production from various mixtures, e.g., Kr–Xe, Xe–N
2
, Xe–O
2
, could be studied. Trace impurities in Xe were analyzed by gas chromatographs with thermal conductivity (TCD), He-ionization (HID), and flame-ionization detectors (FID). Water vapor in the analyzed gases was measured using laseroptical and coulometric hygrometers. The first runs showed that the unit could produce Xe of purity up to 99.9999 %. Experimental data for rectification of Xe to a purity of 99.999 % are presented. Xe could be purified experimentally from traces of CF
4
, C
2
F
6
, SF
6
, hydrocarbons, CO
2
, and H
2
to 0.05; O
2
and N
2
, 0.1; Kr, 0.01; and water vapor, 0.2 ppm.</description><identifier>ISSN: 0009-2355</identifier><identifier>EISSN: 1573-8329</identifier><identifier>DOI: 10.1007/s10556-019-00554-4</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Adsorptivity ; Backup software ; Catalysis ; Chemical plants ; Chemistry ; Chemistry and Materials Science ; Coulometers ; Detection equipment ; Flame ionization detectors ; Gas chromatography ; Geotechnical Engineering & Applied Earth Sciences ; Hygrometers ; Industrial Chemistry/Chemical Engineering ; Industrial Pollution Prevention ; Ionization ; Mineral Resources ; Particle physics ; Physics research ; Purity ; Raw materials ; Technology ; Thermal conductivity ; Trace impurities ; Water vapor ; Xenon</subject><ispartof>Chemical and petroleum engineering, 2019-03, Vol.54 (11-12), p.806-814</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2019</rights><rights>COPYRIGHT 2019 Springer</rights><rights>Copyright Springer Nature B.V. 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c429t-ce241672e1c34f93a9cb0e39cea826b6903da2ccc7f77181744c9d294f5e1fa23</citedby><cites>FETCH-LOGICAL-c429t-ce241672e1c34f93a9cb0e39cea826b6903da2ccc7f77181744c9d294f5e1fa23</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,777,781,27905,27906</link.rule.ids></links><search><creatorcontrib>Bondarenko, V. L.</creatorcontrib><creatorcontrib>Kupriyanov, M. Yu</creatorcontrib><creatorcontrib>Ustyugova, T. G.</creatorcontrib><creatorcontrib>Verkhovnyi, A. I.</creatorcontrib><creatorcontrib>Stefanovskii, A. N.</creatorcontrib><title>Universal Research Cryogenic Unit for Xenon Production</title><title>Chemical and petroleum engineering</title><addtitle>Chem Petrol Eng</addtitle><description>Xenon is a cryogenic product that is currently in short supply. Requirements for its purity are increasing. Its consumption in microelectronics, medicine, and space technology and for high-energy particle physics research is rising. The permissible impurity contents in Xe for various applications were analyzed. A universal research cryogenic unit for Xe production of throughput up to 10 Nm
3
/h of feedstock mixture was designed. A scheme with separation by rectification and preliminary catalytic and adsorptive purification of the feedstock was chosen. The unit was built in blocks so that processing schemes for Xe production from various mixtures, e.g., Kr–Xe, Xe–N
2
, Xe–O
2
, could be studied. Trace impurities in Xe were analyzed by gas chromatographs with thermal conductivity (TCD), He-ionization (HID), and flame-ionization detectors (FID). Water vapor in the analyzed gases was measured using laseroptical and coulometric hygrometers. The first runs showed that the unit could produce Xe of purity up to 99.9999 %. Experimental data for rectification of Xe to a purity of 99.999 % are presented. Xe could be purified experimentally from traces of CF
4
, C
2
F
6
, SF
6
, hydrocarbons, CO
2
, and H
2
to 0.05; O
2
and N
2
, 0.1; Kr, 0.01; and water vapor, 0.2 ppm.</description><subject>Adsorptivity</subject><subject>Backup software</subject><subject>Catalysis</subject><subject>Chemical plants</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Coulometers</subject><subject>Detection equipment</subject><subject>Flame ionization detectors</subject><subject>Gas chromatography</subject><subject>Geotechnical Engineering & Applied Earth Sciences</subject><subject>Hygrometers</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Industrial Pollution Prevention</subject><subject>Ionization</subject><subject>Mineral Resources</subject><subject>Particle physics</subject><subject>Physics research</subject><subject>Purity</subject><subject>Raw materials</subject><subject>Technology</subject><subject>Thermal conductivity</subject><subject>Trace impurities</subject><subject>Water vapor</subject><subject>Xenon</subject><issn>0009-2355</issn><issn>1573-8329</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp9kMtKAzEUhoMoWKsv4GrAlYupuc2kWZbipVBQqgV3Ic2cjFPapCYzYt_e1BHEjWRxkpPvPwkfQpcEjwjG4iYSXBRljonMcdrxnB-hASkEy8eMymM0wBjLnLKiOEVnMa4PR0HpAJVL13xAiHqTLSCCDuYtm4a9r8E1JkuXbWZ9yF7BeZc9BV91pm28O0cnVm8iXPzUIVre3b5MH_L54_1sOpnnhlPZ5gYoJ6WgQAzjVjItzQoDkwb0mJarUmJWaWqMEVYIMiaCcyMrKrktgFhN2RBd9XN3wb93EFu19l1w6UlFKaEizSYiUaOeqvUGVOOsb4M2aVWwbYx3YJvUnxQHF4zRMgWu_wQS08JnW-suRjV7Xvxlac-a4GMMYNUuNFsd9opgdZCvevkqyVff8hVPIdaHYoJdDeH33_-kvgD5pIT0</recordid><startdate>20190301</startdate><enddate>20190301</enddate><creator>Bondarenko, V. L.</creator><creator>Kupriyanov, M. Yu</creator><creator>Ustyugova, T. G.</creator><creator>Verkhovnyi, A. I.</creator><creator>Stefanovskii, A. N.</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>20190301</creationdate><title>Universal Research Cryogenic Unit for Xenon Production</title><author>Bondarenko, V. L. ; Kupriyanov, M. Yu ; Ustyugova, T. G. ; Verkhovnyi, A. I. ; Stefanovskii, A. N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c429t-ce241672e1c34f93a9cb0e39cea826b6903da2ccc7f77181744c9d294f5e1fa23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Adsorptivity</topic><topic>Backup software</topic><topic>Catalysis</topic><topic>Chemical plants</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Coulometers</topic><topic>Detection equipment</topic><topic>Flame ionization detectors</topic><topic>Gas chromatography</topic><topic>Geotechnical Engineering & Applied Earth Sciences</topic><topic>Hygrometers</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Industrial Pollution Prevention</topic><topic>Ionization</topic><topic>Mineral Resources</topic><topic>Particle physics</topic><topic>Physics research</topic><topic>Purity</topic><topic>Raw materials</topic><topic>Technology</topic><topic>Thermal conductivity</topic><topic>Trace impurities</topic><topic>Water vapor</topic><topic>Xenon</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bondarenko, V. L.</creatorcontrib><creatorcontrib>Kupriyanov, M. Yu</creatorcontrib><creatorcontrib>Ustyugova, T. G.</creatorcontrib><creatorcontrib>Verkhovnyi, A. I.</creatorcontrib><creatorcontrib>Stefanovskii, A. N.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Chemical and petroleum engineering</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bondarenko, V. L.</au><au>Kupriyanov, M. Yu</au><au>Ustyugova, T. G.</au><au>Verkhovnyi, A. I.</au><au>Stefanovskii, A. N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Universal Research Cryogenic Unit for Xenon Production</atitle><jtitle>Chemical and petroleum engineering</jtitle><stitle>Chem Petrol Eng</stitle><date>2019-03-01</date><risdate>2019</risdate><volume>54</volume><issue>11-12</issue><spage>806</spage><epage>814</epage><pages>806-814</pages><issn>0009-2355</issn><eissn>1573-8329</eissn><abstract>Xenon is a cryogenic product that is currently in short supply. Requirements for its purity are increasing. Its consumption in microelectronics, medicine, and space technology and for high-energy particle physics research is rising. The permissible impurity contents in Xe for various applications were analyzed. A universal research cryogenic unit for Xe production of throughput up to 10 Nm
3
/h of feedstock mixture was designed. A scheme with separation by rectification and preliminary catalytic and adsorptive purification of the feedstock was chosen. The unit was built in blocks so that processing schemes for Xe production from various mixtures, e.g., Kr–Xe, Xe–N
2
, Xe–O
2
, could be studied. Trace impurities in Xe were analyzed by gas chromatographs with thermal conductivity (TCD), He-ionization (HID), and flame-ionization detectors (FID). Water vapor in the analyzed gases was measured using laseroptical and coulometric hygrometers. The first runs showed that the unit could produce Xe of purity up to 99.9999 %. Experimental data for rectification of Xe to a purity of 99.999 % are presented. Xe could be purified experimentally from traces of CF
4
, C
2
F
6
, SF
6
, hydrocarbons, CO
2
, and H
2
to 0.05; O
2
and N
2
, 0.1; Kr, 0.01; and water vapor, 0.2 ppm.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10556-019-00554-4</doi><tpages>9</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0009-2355 |
| ispartof | Chemical and petroleum engineering, 2019-03, Vol.54 (11-12), p.806-814 |
| issn | 0009-2355 1573-8329 |
| language | eng |
| recordid | cdi_proquest_journals_2212767217 |
| source | Springer Nature |
| subjects | Adsorptivity Backup software Catalysis Chemical plants Chemistry Chemistry and Materials Science Coulometers Detection equipment Flame ionization detectors Gas chromatography Geotechnical Engineering & Applied Earth Sciences Hygrometers Industrial Chemistry/Chemical Engineering Industrial Pollution Prevention Ionization Mineral Resources Particle physics Physics research Purity Raw materials Technology Thermal conductivity Trace impurities Water vapor Xenon |
| title | Universal Research Cryogenic Unit for Xenon Production |
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