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Study of the Specific Features of Kinetics Formation and Structure of the Superconducting Nb3Sn Phase in Technical Superconductors

The growth kinetics of a layer of intermetallic compound Nb 3 Sn in bronze-processed multifilamentary superconductors of different designs and diameters, developed and fabricated at the A.A. Bochvar High-Technology Research Institute of Inorganic Materials (JSC “VNIINM”), has been studied. The influ...

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Published in:Crystallography reports 2019-03, Vol.64 (2), p.252-259
Main Authors: Dergunova, E. A., Karateev, I. A., Vasiliev, A. L., Mareev, K. A., Kurilkin, M. O., Tsapleva, A. S., Abdyukhanov, I. M., Alekseev, M. V., Lomov, A. V.
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container_title Crystallography reports
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creator Dergunova, E. A.
Karateev, I. A.
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Alekseev, M. V.
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description The growth kinetics of a layer of intermetallic compound Nb 3 Sn in bronze-processed multifilamentary superconductors of different designs and diameters, developed and fabricated at the A.A. Bochvar High-Technology Research Institute of Inorganic Materials (JSC “VNIINM”), has been studied. The influence of diffusion annealing conditions in a wide range of temperatures and exposure times on the formation of Nb 3 Sn phase in superconductors has been investigated by methods of metallographic analysis using optical microscopy, electron microscopy, and microanalysis. The structural features of Nb 3 Sn layers in the initial formation stage and after long-term diffusion annealing are analyzed, their thickness is measured, and the grain structure and composition are studied. Recommendations on improvement of the diffusion annealing conditions for Nb 3 Sn superconductors of different designs, aimed at obtaining high current-carrying ability, are elaborated.
doi_str_mv 10.1134/S1063774519020093
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subjects Annealing
Crystallography and Scattering Methods
Diffusion annealing
Diffusion layers
Grain structure
Inorganic materials
Intermetallic compounds
Microscopy
Optical microscopy
Physics
Physics and Astronomy
Structure of Inorganic Compounds
Thickness measurement
title Study of the Specific Features of Kinetics Formation and Structure of the Superconducting Nb3Sn Phase in Technical Superconductors
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