Microstructure and mechanical properties of severely deformed Al-Mg-Sc-Zr alloy and their evolution during annealing

• Published in: Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2019-04, Vol.754, p.295-308
• Main Authors: Tang, Lei, Peng, Xiaoyan, Huang, Jiwu, Ma, Aibin, Deng, Ying, Xu, Guofu
• Format: Article
• Language: English
• Subjects: Al-Mg-Sc-Zr; Aluminum base alloys; Annealing; Anti-recrystallization; Cold pressing; Cold rolling; Dislocation density; ECAP; Electron backscatter diffraction; Elongation; Equal channel angular pressing; Evolution; Grain structure; High temperature; Inhomogeneity; Magnesium; Mechanical properties; Microstructure; Plastic deformation; Scandium; Transmission electron microscopy; Ultrafine grains; Ultrafines; X-ray diffraction; Yield strength; Zirconium base alloys
• ISSN: 0921-5093; 1873-4936
• DOI: 10.1016/j.msea.2018.12.063

The ultrafine-grained structure developed here after severe plastic deformation of Al-Mg and Al-Mg-Sc-Zr by equal channel angular pressing (ECAP) and cold rolling (CR) is presented to consist of dense dislocation walls and cell structure of dimension of ~ 300 nm. Detailed characterization by traditional transmission electron microscopy (TEM), electron backscattered diffraction (EBSD) and X-ray diffraction (XRD) has been carried out to reveal microstructure evolution during deformation and annealing. A unique bimodal grain structure, which consists of ultrafine grains (less than 150 nm) and fine grains (in the range of 200–500 nm) having high dislocation density, was developed after 16 ECAP passes and CR. It was also found that microstructure inhomogeneity exits even after high ECAP passes and annealing at high temperature (280 °C) for 1 h. High yield strength (YS) of ~ 550 MPa and tensile strength (TS) of ~ 560 MPa were obtained after 16 ECAP passes and CR, however, the corresponding elongation dropped to ~ 8.2%. Subsequent optimum annealing was found to be 240 °C × 1 h, by which comprehensive mechanical properties were maintained (~ 481 MPa for YS, ~ 512 MPa for TS and ~ 13.7% for elongation) in Al-Mg-Sc-Zr (16 ECAP passes). The reasons of inhomogeneous microstructure and the origins of high strength, i.e. high solute Mg content, dense dislocations, ultrafine grains and nanoscale Al3(Sc, Zr) particles are discussed.