Relationship between Strength in Magnetic Field and Spectral Width of Solid-state 33S NMR in an Organosulfur Compound

Correlation between strength in an external magnetic field and spectral width of solid-state sulfur-33 nuclear magnetic resonance (NMR) spectra in an organosulfur compound, whose quadrupolar coupling constant is more than 40 MHz, is discussed. As an alternative method to higher magnetic field NMR, W...

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Bibliographic Details
Published in:Chemistry letters 2019-06, Vol.48 (6), p.601-603
Main Authors: Yamada, Kazuhiko, Ohki, Shinobu, Deguchi, Kenzo, Hashi, Kenjiro, Goto, Atsushi, Shimizu, Tadashi
Format: Article
Language:eng ; jpn
Subjects:
Coupling (molecular)
Magnetic fields
Magnetism
NMR
Nuclear magnetic resonance
Organosulfur compounds
Solid state
Spectra
Sulfur isotopes
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Summary:Correlation between strength in an external magnetic field and spectral width of solid-state sulfur-33 nuclear magnetic resonance (NMR) spectra in an organosulfur compound, whose quadrupolar coupling constant is more than 40 MHz, is discussed. As an alternative method to higher magnetic field NMR, WURST-QCPMG technique at lower magnetic field is proposed and the result is presented.
ISSN:0366-7022
1348-0715
DOI:10.1246/cl.190102