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Structural and thermal studies of SmNbO4 polymorphs produced by mechanical alloying
[Display omitted] •High temperature SmNbO4 phase was synthetized at room temperature.•The high temperature phase is stable at least 800 °C.•A single SmNbO4 nanostructured phase was obtained with annealing at 1000 °C. A nanostructured mixture of two SmNbO4 polymorphs, one monoclinic and other tetrago...
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Published in: | Materials letters 2019-10, Vol.252, p.313-316 |
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creator | de Brito Neto, Francisco Maciel Takeno, Mitsuo Lopes da Costa Pinto, Camila Trichês, Daniela Menegon Manzato, Lizandro Michielon de Souza, Sérgio |
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•High temperature SmNbO4 phase was synthetized at room temperature.•The high temperature phase is stable at least 800 °C.•A single SmNbO4 nanostructured phase was obtained with annealing at 1000 °C.
A nanostructured mixture of two SmNbO4 polymorphs, one monoclinic and other tetragonal, was synthesized by mechanical alloying. It was the first time that the tetragonal structure was synthesized at low temperature. Both polymorphs are stable in high temperatures. A single monoclinic phase with nanometric crystallites was obtained after annealing at 1000 °C. |
doi_str_mv | 10.1016/j.matlet.2019.06.004 |
format | article |
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•High temperature SmNbO4 phase was synthetized at room temperature.•The high temperature phase is stable at least 800 °C.•A single SmNbO4 nanostructured phase was obtained with annealing at 1000 °C.
A nanostructured mixture of two SmNbO4 polymorphs, one monoclinic and other tetragonal, was synthesized by mechanical alloying. It was the first time that the tetragonal structure was synthesized at low temperature. Both polymorphs are stable in high temperatures. A single monoclinic phase with nanometric crystallites was obtained after annealing at 1000 °C.</description><identifier>ISSN: 0167-577X</identifier><identifier>EISSN: 1873-4979</identifier><identifier>DOI: 10.1016/j.matlet.2019.06.004</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Crystallites ; Materials science ; Mechanical alloying ; Rare-Earth ; Rietveld method ; Synthesis ; X-ray diffraction</subject><ispartof>Materials letters, 2019-10, Vol.252, p.313-316</ispartof><rights>2019</rights><rights>Copyright Elsevier BV Oct 1, 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c334t-ef269c182cce585891fb560de7f8327eab0243c9d6e11a4d4d362466195147c43</citedby><cites>FETCH-LOGICAL-c334t-ef269c182cce585891fb560de7f8327eab0243c9d6e11a4d4d362466195147c43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>de Brito Neto, Francisco Maciel</creatorcontrib><creatorcontrib>Takeno, Mitsuo Lopes</creatorcontrib><creatorcontrib>da Costa Pinto, Camila</creatorcontrib><creatorcontrib>Trichês, Daniela Menegon</creatorcontrib><creatorcontrib>Manzato, Lizandro</creatorcontrib><creatorcontrib>Michielon de Souza, Sérgio</creatorcontrib><title>Structural and thermal studies of SmNbO4 polymorphs produced by mechanical alloying</title><title>Materials letters</title><description>[Display omitted]
•High temperature SmNbO4 phase was synthetized at room temperature.•The high temperature phase is stable at least 800 °C.•A single SmNbO4 nanostructured phase was obtained with annealing at 1000 °C.
A nanostructured mixture of two SmNbO4 polymorphs, one monoclinic and other tetragonal, was synthesized by mechanical alloying. It was the first time that the tetragonal structure was synthesized at low temperature. Both polymorphs are stable in high temperatures. A single monoclinic phase with nanometric crystallites was obtained after annealing at 1000 °C.</description><subject>Crystallites</subject><subject>Materials science</subject><subject>Mechanical alloying</subject><subject>Rare-Earth</subject><subject>Rietveld method</subject><subject>Synthesis</subject><subject>X-ray diffraction</subject><issn>0167-577X</issn><issn>1873-4979</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp9kEtLxDAUhYMoOI7-AxcF161JkybtRhDxBYOzGAV3IU1unZQ-xiQV-u_NUNeu7l2cc-49H0LXBGcEE37bZr0KHYQsx6TKMM8wZidoRUpBU1aJ6hStokykhRCf5-jC-xZHRYXZCu12wU06TE51iRpMEvbg-rj7MBkLPhmbZNe_1VuWHMZu7kd32Pvk4EYzaTBJPSc96L0arD76u26c7fB1ic4a1Xm4-ptr9PH0-P7wkm62z68P95tUU8pCCk3OK03KXGsoyqKsSFMXHBsQTUlzAarGOaO6MhwIUcwwQ3nOOCdVQZjQjK7RzZIb__mewAfZjpMb4kmZ54IKFiNFVLFFpd3ovYNGHpztlZslwfKIT7ZywSeP-CTmMsKJtrvFBrHBjwUnvbYwxNbWgQ7SjPb_gF8hQ3ra</recordid><startdate>20191001</startdate><enddate>20191001</enddate><creator>de Brito Neto, Francisco Maciel</creator><creator>Takeno, Mitsuo Lopes</creator><creator>da Costa Pinto, Camila</creator><creator>Trichês, Daniela Menegon</creator><creator>Manzato, Lizandro</creator><creator>Michielon de Souza, Sérgio</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20191001</creationdate><title>Structural and thermal studies of SmNbO4 polymorphs produced by mechanical alloying</title><author>de Brito Neto, Francisco Maciel ; Takeno, Mitsuo Lopes ; da Costa Pinto, Camila ; Trichês, Daniela Menegon ; Manzato, Lizandro ; Michielon de Souza, Sérgio</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c334t-ef269c182cce585891fb560de7f8327eab0243c9d6e11a4d4d362466195147c43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Crystallites</topic><topic>Materials science</topic><topic>Mechanical alloying</topic><topic>Rare-Earth</topic><topic>Rietveld method</topic><topic>Synthesis</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>de Brito Neto, Francisco Maciel</creatorcontrib><creatorcontrib>Takeno, Mitsuo Lopes</creatorcontrib><creatorcontrib>da Costa Pinto, Camila</creatorcontrib><creatorcontrib>Trichês, Daniela Menegon</creatorcontrib><creatorcontrib>Manzato, Lizandro</creatorcontrib><creatorcontrib>Michielon de Souza, Sérgio</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>de Brito Neto, Francisco Maciel</au><au>Takeno, Mitsuo Lopes</au><au>da Costa Pinto, Camila</au><au>Trichês, Daniela Menegon</au><au>Manzato, Lizandro</au><au>Michielon de Souza, Sérgio</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structural and thermal studies of SmNbO4 polymorphs produced by mechanical alloying</atitle><jtitle>Materials letters</jtitle><date>2019-10-01</date><risdate>2019</risdate><volume>252</volume><spage>313</spage><epage>316</epage><pages>313-316</pages><issn>0167-577X</issn><eissn>1873-4979</eissn><abstract>[Display omitted]
•High temperature SmNbO4 phase was synthetized at room temperature.•The high temperature phase is stable at least 800 °C.•A single SmNbO4 nanostructured phase was obtained with annealing at 1000 °C.
A nanostructured mixture of two SmNbO4 polymorphs, one monoclinic and other tetragonal, was synthesized by mechanical alloying. It was the first time that the tetragonal structure was synthesized at low temperature. Both polymorphs are stable in high temperatures. A single monoclinic phase with nanometric crystallites was obtained after annealing at 1000 °C.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.matlet.2019.06.004</doi><tpages>4</tpages></addata></record> |
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subjects | Crystallites Materials science Mechanical alloying Rare-Earth Rietveld method Synthesis X-ray diffraction |
title | Structural and thermal studies of SmNbO4 polymorphs produced by mechanical alloying |
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