Simple, efficient, and eco‐friendly sample preparation for simultaneous determination of paracetamol and chloramphenicol in meat

We have developed and validated a simple, eco‐friendly, and reliable method to simultaneously determine paracetamol and chloramphenicol in meat with ultra performance liquid chromatography and tandem mass spectrometry. The samples were firstly extracted with ethylenediaminetetraacetic acid–McIlvaine...

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Bibliographic Details
Published in:Journal of separation science 2019-08, Vol.42 (16), p.2696-2705
Main Authors: Jian, Ningge, Li, Ruixian, Li, Jian, Liang, Sihui, Xu, Qian, Wang, Chunmin
Format: Article
Language:English
Subjects:
Acetaminophen - analysis
Analgesics
Analytical chemistry
Animals
Cattle
Chickens
chloramphenicol
Chloramphenicol - analysis
Chloromycetin
Chromatography, High Pressure Liquid
Food Contamination - analysis
Ions
Liquid chromatography
Mass spectrometry
Meat
Meat - analysis
Nanofibers
nanofibers mat
paracetamol
Polyacrylonitrile
Polyanilines
Pork
Solid Phase Extraction
Swine
Tandem Mass Spectrometry
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Summary:We have developed and validated a simple, eco‐friendly, and reliable method to simultaneously determine paracetamol and chloramphenicol in meat with ultra performance liquid chromatography and tandem mass spectrometry. The samples were firstly extracted with ethylenediaminetetraacetic acid–McIlvaine's buffer and then purified by solid‐phase extraction by using a novel core‐shell polyaniline/polyacrylonitrile nanofibers mat. Compared with existing methods for the two analytes, the proposed method was simplified greatly with much fewer sample preparation steps, consumed much less time (
ISSN:1615-9306
1615-9314
DOI:10.1002/jssc.201900224