Oxidation Behavior Across Composition Space Relevant to Co-based γ/γ′ Alloys

A multi-source ion-plasma deposition technique was used to create a series of three combinatorial libraries across the Co-Ni-Al-W-Cr-Ta composition space relevant to the formation of Co-based γ / γ ′ microstructures. Alloys were isothermally oxidized for 1 hour in air at 1100 °C, and screened for Al...

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Published in:Metallurgical and materials transactions. A, Physical metallurgy and materials science Physical metallurgy and materials science, 2019-11, Vol.50 (11), p.5445-5458
Main Authors: Stewart, Colin A., Suzuki, Akane, Rhein, Robert K., Pollock, Tresa M., Levi, Carlos G.
Format: Article
Language:English
Subjects:
Aluminum oxide
Characterization and Evaluation of Materials
Chemistry and Materials Science
Chromium
Combinatorial analysis
Composition
Materials Science
Metallic Materials
Nanotechnology
Nickel base alloys
Oxidation
Plasma deposition
Scale formation
Structural Materials
Superalloys
Surfaces and Interfaces
Thin Films
Tungsten
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container_end_page 5458
container_issue 11
container_start_page 5445
container_title Metallurgical and materials transactions. A, Physical metallurgy and materials science
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creator Stewart, Colin A.
Suzuki, Akane
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Pollock, Tresa M.
Levi, Carlos G.
description A multi-source ion-plasma deposition technique was used to create a series of three combinatorial libraries across the Co-Ni-Al-W-Cr-Ta composition space relevant to the formation of Co-based γ / γ ′ microstructures. Alloys were isothermally oxidized for 1 hour in air at 1100 °C, and screened for Al 2 O 3 scale formation using a high-throughput photo-stimulated luminescence spectroscopy technique. Select compositions were then analyzed in cross-section via EDS in the SEM and TEM. The resulting oxide microstructures are presented, and paths to explain their evolution are proposed. Compositions forming α-Al 2 O 3 with thinner amounts of overlying oxides are highlighted. The thinnest scale observed was ~ 1  μ m, comparable to second-generation Ni-base superalloys oxidized under the same conditions.
doi_str_mv 10.1007/s11661-019-05413-8
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subjects Aluminum oxide
Characterization and Evaluation of Materials
Chemistry and Materials Science
Chromium
Combinatorial analysis
Composition
Materials Science
Metallic Materials
Nanotechnology
Nickel base alloys
Oxidation
Plasma deposition
Scale formation
Structural Materials
Superalloys
Surfaces and Interfaces
Thin Films
Tungsten
title Oxidation Behavior Across Composition Space Relevant to Co-based γ/γ′ Alloys
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