Grain refinement and superplastic flow in friction stir processed Ti–15V–3Cr–3Sn–3Al alloy

• Published in: Journal of alloys and compounds 2019-09, Vol.803, p.901-911
• Main Authors: Zhang, Wenjing, Liu, Huihong, Ding, Hua, Fujii, Hidetoshi
• Format: Article
• Language: English
• Subjects: Continuous dynamic recrystallization; Deformation mechanisms; Dislocations; Dynamic recrystallization; Elongation; Friction stir processing; Grain boundaries; Grain boundaries sliding; Grain growth; Grain refinement; Grain size; Low-temperature superplasticity; Microstructure; Plastic deformation; Superplastic deformation; Superplastic forming; Superplasticity; Tensile tests; Ti-15-3 alloy; Titanium alloys; Titanium base alloys
• ISSN: 0925-8388; 1873-4669
• DOI: 10.1016/j.jallcom.2019.06.323

The rolled Ti–15V–3Cr–3Sn–3Al (Ti-15-3) alloy (metastable β titanium alloy) sheet with an average grain size of 44.0 μm was subjected to friction stir processing (FSP) at a tool rotation speed of 250 rpm and a tool traverse speed of 100 mm/min (250–100). Thereafter, a fine-grained (∼6.6 μm) and relatively equiaxed microstructure with a high angle grain boundary (HAGB) ratio of 74.5% was observed in the stir zone (SZ). Superplastic tensile tests were then conducted on this microstructure at the temperatures ranging from 600 °C to 800 °C and strain rates range of 1 × 10−4-1 × 10−2 s−1, and an excellent low-temperature superplasticity (LTSP) with the elongation of 463% was obtained at 650 °C and 1 × 10−4 s−1. In addition, the microstructure in the gauge section of the tensile specimens interrupted at different engineering strains of 20%, 50%, 200%, and 463% (tensile fractured) at the optimal superplastic tensile condition of 650 °C and 1 × 10−4 s−1 was studied. It was found that the precipitated α phase increased with the increasing strain, which contributed to the achievement of an enhanced LTSP by inhibiting the grain growth. Moreover, the α grains with a finer grain size of 4.4 μm was observed in the gauge section of the tensile fractured specimen and this was attributed to the occurrence of continuous dynamic recrystallization (CDRX). Therefore, the superplastic deformation mechanism of the Ti-15-3 alloy is recognized as grain boundaries sliding (GBS) accompanied with dislocation movement and CDRX at 650 °C and 1 × 10−4 s−1. •It is the first time to report the study on the superplasticity in the friction stir processed Ti-15-3 alloy.•The 6.6 μm-grained equiaxed microstructure was obtained in the friction stir processed Ti-15-3 alloy.•The largest elongation of 463% was achieved in the friction stir processed Ti-15-3 alloy at the low temperature of 650 °C.•The precipitated α phase during tensile deformation can effectively inhibit the severe grain growth.•The superior superplastic properties were mainly attributed to the precipitated α phase during tensile deformation.