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Multicomponent one-pot synthesis of (dihydro-1H-benzo[d]imidazole) phosphonate
We present a multicomponent reaction strategy to synthesize a (dihydro-1H-benzo[d]imidazole)phosphonate family of compounds, using benzimidazoles, diethyl chlorophosphate and aliphatic amines as starting reactants. Giving its simplicity, our procedure involves reaction times of only few hours and av...
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| Published in: | Phosphorus, sulfur, and silicon and the related elements sulfur, and silicon and the related elements, 2019-11, Vol.194 (11), p.1062-1066 |
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| Main Authors: | , , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c338t-1770be8f8a012eba597271a1989bae33f05d4c0e141e602fb325d02768532b853 |
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| cites | cdi_FETCH-LOGICAL-c338t-1770be8f8a012eba597271a1989bae33f05d4c0e141e602fb325d02768532b853 |
| container_end_page | 1066 |
| container_issue | 11 |
| container_start_page | 1062 |
| container_title | Phosphorus, sulfur, and silicon and the related elements |
| container_volume | 194 |
| creator | Castrejon-Flores, José Luis Guevara-Moreno, Oscar Ernesto Díaz-Contreras, Raúl Ricardo Gutiérrez-Carrillo, Atilano Franco-Pérez, Marco Suárez-Moreno, Galdina Vanessa Zamudio-Medina, Angel |
| description | We present a multicomponent reaction strategy to synthesize a (dihydro-1H-benzo[d]imidazole)phosphonate family of compounds, using benzimidazoles, diethyl chlorophosphate and aliphatic amines as starting reactants. Giving its simplicity, our procedure involves reaction times of only few hours and avoid the usage of any catalyst agent. All the newly synthesized compounds were characterized by Nuclear Magnetic Resonance spectroscopy (
1
H,
13
C and
31
P) and mass spectrometry by the DART method. |
| doi_str_mv | 10.1080/10426507.2019.1602834 |
| format | article |
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1
H,
13
C and
31
P) and mass spectrometry by the DART method.</description><identifier>ISSN: 1042-6507</identifier><identifier>EISSN: 1563-5325</identifier><identifier>DOI: 10.1080/10426507.2019.1602834</identifier><language>eng</language><publisher>Abingdon: Taylor & Francis</publisher><subject>Aliphatic amines ; Amines ; benzimidazoles ; Chemical synthesis ; diethyl chlorophosphate ; Imidazole ; Mass spectrometry ; Multicomponent reactions ; NMR ; Nuclear magnetic resonance ; Phosphonates</subject><ispartof>Phosphorus, sulfur, and silicon and the related elements, 2019-11, Vol.194 (11), p.1062-1066</ispartof><rights>2019 Taylor & Francis Group, LLC 2019</rights><rights>2019 Taylor & Francis Group, LLC</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c338t-1770be8f8a012eba597271a1989bae33f05d4c0e141e602fb325d02768532b853</citedby><cites>FETCH-LOGICAL-c338t-1770be8f8a012eba597271a1989bae33f05d4c0e141e602fb325d02768532b853</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,778,782,27911,27912</link.rule.ids></links><search><creatorcontrib>Castrejon-Flores, José Luis</creatorcontrib><creatorcontrib>Guevara-Moreno, Oscar Ernesto</creatorcontrib><creatorcontrib>Díaz-Contreras, Raúl Ricardo</creatorcontrib><creatorcontrib>Gutiérrez-Carrillo, Atilano</creatorcontrib><creatorcontrib>Franco-Pérez, Marco</creatorcontrib><creatorcontrib>Suárez-Moreno, Galdina Vanessa</creatorcontrib><creatorcontrib>Zamudio-Medina, Angel</creatorcontrib><title>Multicomponent one-pot synthesis of (dihydro-1H-benzo[d]imidazole) phosphonate</title><title>Phosphorus, sulfur, and silicon and the related elements</title><description>We present a multicomponent reaction strategy to synthesize a (dihydro-1H-benzo[d]imidazole)phosphonate family of compounds, using benzimidazoles, diethyl chlorophosphate and aliphatic amines as starting reactants. Giving its simplicity, our procedure involves reaction times of only few hours and avoid the usage of any catalyst agent. All the newly synthesized compounds were characterized by Nuclear Magnetic Resonance spectroscopy (
1
H,
13
C and
31
P) and mass spectrometry by the DART method.</description><subject>Aliphatic amines</subject><subject>Amines</subject><subject>benzimidazoles</subject><subject>Chemical synthesis</subject><subject>diethyl chlorophosphate</subject><subject>Imidazole</subject><subject>Mass spectrometry</subject><subject>Multicomponent reactions</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Phosphonates</subject><issn>1042-6507</issn><issn>1563-5325</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp9UE1LAzEUDKJgrf4EYcGLHlJfkv28KUWtUPWiJ5GQ3U1oym6yJimy_fWmtF49vHnvMDOPGYQuCcwIlHBLIKV5BsWMAqlmJAdasvQITUiWM5wxmh3HO3LwjnSKzrxfA0BFGUzQ68umC7qx_WCNNCGJiAcbEj-asJJe-8Sq5LrVq7F1FpMFrqXZ2s_2S_e6FVvbyZtkWFkfx4ggz9GJEp2XF4c9RR-PD-_zBV6-PT3P75e4YawMmBQF1LJUpQBCZS2yqqAFEaQqq1pIxhRkbdqAJCmRMY6qY4gWaJGXMU4dYYqu9r6Ds98b6QNf240z8SWPsSDNipySyMr2rMZZ751UfHC6F27kBPiuOv5XHd9Vxw_VRd3dXqeNsq4XP9Z1LQ9i7KxTTphGe87-t_gFtPB0gA</recordid><startdate>20191102</startdate><enddate>20191102</enddate><creator>Castrejon-Flores, José Luis</creator><creator>Guevara-Moreno, Oscar Ernesto</creator><creator>Díaz-Contreras, Raúl Ricardo</creator><creator>Gutiérrez-Carrillo, Atilano</creator><creator>Franco-Pérez, Marco</creator><creator>Suárez-Moreno, Galdina Vanessa</creator><creator>Zamudio-Medina, Angel</creator><general>Taylor & Francis</general><general>Taylor & Francis Ltd</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20191102</creationdate><title>Multicomponent one-pot synthesis of (dihydro-1H-benzo[d]imidazole) phosphonate</title><author>Castrejon-Flores, José Luis ; Guevara-Moreno, Oscar Ernesto ; Díaz-Contreras, Raúl Ricardo ; Gutiérrez-Carrillo, Atilano ; Franco-Pérez, Marco ; Suárez-Moreno, Galdina Vanessa ; Zamudio-Medina, Angel</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c338t-1770be8f8a012eba597271a1989bae33f05d4c0e141e602fb325d02768532b853</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Aliphatic amines</topic><topic>Amines</topic><topic>benzimidazoles</topic><topic>Chemical synthesis</topic><topic>diethyl chlorophosphate</topic><topic>Imidazole</topic><topic>Mass spectrometry</topic><topic>Multicomponent reactions</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Phosphonates</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Castrejon-Flores, José Luis</creatorcontrib><creatorcontrib>Guevara-Moreno, Oscar Ernesto</creatorcontrib><creatorcontrib>Díaz-Contreras, Raúl Ricardo</creatorcontrib><creatorcontrib>Gutiérrez-Carrillo, Atilano</creatorcontrib><creatorcontrib>Franco-Pérez, Marco</creatorcontrib><creatorcontrib>Suárez-Moreno, Galdina Vanessa</creatorcontrib><creatorcontrib>Zamudio-Medina, Angel</creatorcontrib><collection>CrossRef</collection><jtitle>Phosphorus, sulfur, and silicon and the related elements</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Castrejon-Flores, José Luis</au><au>Guevara-Moreno, Oscar Ernesto</au><au>Díaz-Contreras, Raúl Ricardo</au><au>Gutiérrez-Carrillo, Atilano</au><au>Franco-Pérez, Marco</au><au>Suárez-Moreno, Galdina Vanessa</au><au>Zamudio-Medina, Angel</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Multicomponent one-pot synthesis of (dihydro-1H-benzo[d]imidazole) phosphonate</atitle><jtitle>Phosphorus, sulfur, and silicon and the related elements</jtitle><date>2019-11-02</date><risdate>2019</risdate><volume>194</volume><issue>11</issue><spage>1062</spage><epage>1066</epage><pages>1062-1066</pages><issn>1042-6507</issn><eissn>1563-5325</eissn><abstract>We present a multicomponent reaction strategy to synthesize a (dihydro-1H-benzo[d]imidazole)phosphonate family of compounds, using benzimidazoles, diethyl chlorophosphate and aliphatic amines as starting reactants. Giving its simplicity, our procedure involves reaction times of only few hours and avoid the usage of any catalyst agent. All the newly synthesized compounds were characterized by Nuclear Magnetic Resonance spectroscopy (
1
H,
13
C and
31
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| identifier | ISSN: 1042-6507 |
| ispartof | Phosphorus, sulfur, and silicon and the related elements, 2019-11, Vol.194 (11), p.1062-1066 |
| issn | 1042-6507 1563-5325 |
| language | eng |
| recordid | cdi_proquest_journals_2300457621 |
| source | Taylor and Francis Science and Technology Collection |
| subjects | Aliphatic amines Amines benzimidazoles Chemical synthesis diethyl chlorophosphate Imidazole Mass spectrometry Multicomponent reactions NMR Nuclear magnetic resonance Phosphonates |
| title | Multicomponent one-pot synthesis of (dihydro-1H-benzo[d]imidazole) phosphonate |
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