Synthesis of Tetrazoles from Amines Mediated by New Copper Nanocatalyst

New copper nanocatalyst was prepared by coating Fe 3 O 4 magnetic nanoparticles with tetraethyl orthosilicate (TEOS), followed by functionalization with 3-chloropropyl(trimethoxy)silane and 4 H -1,2,4-tri-azol-4-amine and complexation with copper(II) chloride. The new catalyst was characterized by v...

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Published in:Russian journal of organic chemistry 2019-10, Vol.55 (10), p.1591-1597
Main Authors: Ariannezhad, M., Habibi, D., Heydari, S.
Format: Article
Language:English
Subjects:
Amines
Aromatic compounds
Chemical synthesis
Chemistry
Chemistry and Materials Science
Copper
Copper compounds
Iron oxides
Nanoparticles
Organic Chemistry
Sodium azides
Tetraethyl orthosilicate
Tetrazoles
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description New copper nanocatalyst was prepared by coating Fe 3 O 4 magnetic nanoparticles with tetraethyl orthosilicate (TEOS), followed by functionalization with 3-chloropropyl(trimethoxy)silane and 4 H -1,2,4-tri-azol-4-amine and complexation with copper(II) chloride. The new catalyst was characterized by various spectroscopic methods and was successfully used in the synthesis of 1-aryl-1 H -tetrazoles by reaction of aromatic amines with sodium azide and triethyl orthoformate under solvent-free conditions at 100°C.
doi_str_mv 10.1134/S1070428019100208
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subjects Amines
Aromatic compounds
Chemical synthesis
Chemistry
Chemistry and Materials Science
Copper
Copper compounds
Iron oxides
Nanoparticles
Organic Chemistry
Sodium azides
Tetraethyl orthosilicate
Tetrazoles
title Synthesis of Tetrazoles from Amines Mediated by New Copper Nanocatalyst
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