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MnSb2O6‐chitosan nanocomposite: An efficient catalyst for the synthesis of coumarins via Pechmann reaction
In this work, MnSb2O6‐chitosan nanocomposites were synthesized and have been employed in Pechmann condensation for the synthesis of coumarin derivatives. MnSb2O6‐chitosan nanocomposites were characterized by Fourier transform infrared (FTIR), X‐ray powder diffraction (XRD), scanning electron microsc...
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Published in: | Journal of heterocyclic chemistry 2020-01, Vol.57 (1), p.173-181 |
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container_title | Journal of heterocyclic chemistry |
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creator | Bahramnezhad, Baharak Ghazanfari, Dadkhoda Sheikhhosseini, Enayatollah Akhgar, Mohammad Reza Ahmadi, Sayed Ali |
description | In this work, MnSb2O6‐chitosan nanocomposites were synthesized and have been employed in Pechmann condensation for the synthesis of coumarin derivatives. MnSb2O6‐chitosan nanocomposites were characterized by Fourier transform infrared (FTIR), X‐ray powder diffraction (XRD), scanning electron microscope (SEM), and energy‐dispersive X‐ray spectroscopy (EDX) techniques. The particles of MnSb2O6‐chitosan have uniform spheres with sizes that are less than 100 nm. Simplicity, easy work‐up, and short reaction times are advantages of this reaction. Also, we evaluated the antibacterial activity for some of the products, and the result showed significant pharmaceutical activities as antibacterial reagents against Staphylococcus aureus and Escherichia coli. |
doi_str_mv | 10.1002/jhet.3763 |
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MnSb2O6‐chitosan nanocomposites were characterized by Fourier transform infrared (FTIR), X‐ray powder diffraction (XRD), scanning electron microscope (SEM), and energy‐dispersive X‐ray spectroscopy (EDX) techniques. The particles of MnSb2O6‐chitosan have uniform spheres with sizes that are less than 100 nm. Simplicity, easy work‐up, and short reaction times are advantages of this reaction. 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Also, we evaluated the antibacterial activity for some of the products, and the result showed significant pharmaceutical activities as antibacterial reagents against Staphylococcus aureus and Escherichia coli.</description><subject>Catalysts</subject><subject>Chemical synthesis</subject><subject>Chitosan</subject><subject>Condensates</subject><subject>Coumarin</subject><subject>E coli</subject><subject>Electron microscopes</subject><subject>Fourier transforms</subject><subject>Nanocomposites</subject><subject>Reagents</subject><issn>0022-152X</issn><issn>1943-5193</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid/><recordid>eNotkN9KwzAUxoMoOKcXvkHA67r8a9N6N8Z0ymSCE7wLaZrQjC6pTab0zkfwGX0SW-bVdw7n4zsfPwCuMbrFCJHZrtbxlvKMnoAJLhhNUlzQUzAZbiTBKXk_Bxch7IYVU84noHl2ryXZZL_fP6q20QfpoJPOK79vfbBR38G5g9oYq6x2ESoZZdOHCI3vYKw1DL0bJNgAvYHKH_aysy7ATyvhi1b1XjoHOy1VtN5dgjMjm6Cv_nUK3u6X28UqWW8eHhfzddISQmlSFZqlFZcllZlCOcIZQykzqEKF0jkueaq4yVOlKlphxjNeapKWJldGo6pSmE7BzTG37fzHQYcodv7QueGlIJSRguW0oINrdnR92Ub3ou3s0L0XGImRpBhJipGkeFott-NA_wBIPGt9</recordid><startdate>202001</startdate><enddate>202001</enddate><creator>Bahramnezhad, Baharak</creator><creator>Ghazanfari, Dadkhoda</creator><creator>Sheikhhosseini, Enayatollah</creator><creator>Akhgar, Mohammad Reza</creator><creator>Ahmadi, Sayed Ali</creator><general>Wiley Subscription Services, Inc</general><scope/><orcidid>https://orcid.org/0000-0003-0148-2462</orcidid><orcidid>https://orcid.org/0000-0003-2973-9768</orcidid></search><sort><creationdate>202001</creationdate><title>MnSb2O6‐chitosan nanocomposite: An efficient catalyst for the synthesis of coumarins via Pechmann reaction</title><author>Bahramnezhad, Baharak ; Ghazanfari, Dadkhoda ; Sheikhhosseini, Enayatollah ; Akhgar, Mohammad Reza ; Ahmadi, Sayed Ali</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p2233-d9e45d7ab3a6c080164054f0d09ce81b75c7f85ccd3d14767be25bf8cfe0ddc13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Catalysts</topic><topic>Chemical synthesis</topic><topic>Chitosan</topic><topic>Condensates</topic><topic>Coumarin</topic><topic>E coli</topic><topic>Electron microscopes</topic><topic>Fourier transforms</topic><topic>Nanocomposites</topic><topic>Reagents</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bahramnezhad, Baharak</creatorcontrib><creatorcontrib>Ghazanfari, Dadkhoda</creatorcontrib><creatorcontrib>Sheikhhosseini, Enayatollah</creatorcontrib><creatorcontrib>Akhgar, Mohammad Reza</creatorcontrib><creatorcontrib>Ahmadi, Sayed Ali</creatorcontrib><jtitle>Journal of heterocyclic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bahramnezhad, Baharak</au><au>Ghazanfari, Dadkhoda</au><au>Sheikhhosseini, Enayatollah</au><au>Akhgar, Mohammad Reza</au><au>Ahmadi, Sayed Ali</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>MnSb2O6‐chitosan nanocomposite: An efficient catalyst for the synthesis of coumarins via Pechmann reaction</atitle><jtitle>Journal of heterocyclic chemistry</jtitle><date>2020-01</date><risdate>2020</risdate><volume>57</volume><issue>1</issue><spage>173</spage><epage>181</epage><pages>173-181</pages><issn>0022-152X</issn><eissn>1943-5193</eissn><abstract>In this work, MnSb2O6‐chitosan nanocomposites were synthesized and have been employed in Pechmann condensation for the synthesis of coumarin derivatives. 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subjects | Catalysts Chemical synthesis Chitosan Condensates Coumarin E coli Electron microscopes Fourier transforms Nanocomposites Reagents |
title | MnSb2O6‐chitosan nanocomposite: An efficient catalyst for the synthesis of coumarins via Pechmann reaction |
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