Dynamic ball indentation for powder flow characterization

• Published in: Powder technology 2020-01, Vol.360, p.1047-1054
• Main Authors: Tirapelle, Monica, Santomaso, Andrea C., Hare, Colin
• Format: Article
• Language: English
• Subjects: Ball indentation; Dynamic flow; Flow; Hardness; High speed cameras; Indentation; Intermediate flow regime; Mixers; Penetration depth; Powder; Powder flowability; Powder rheology; Rheological properties; Screw conveyors; Strain rate; Yield stress
• ISSN: 0032-5910; 1873-328X
• DOI: 10.1016/j.powtec.2019.11.009

In industrial processing and manufacturing, characterizing the flowability of particulate solids is of particular importance both for reliable powder flow and for a consistent production rate. Shear testing is the most widely used method for powders subjected to moderate or high stresses, and under quasi-static conditions. However, this method is not suitable for measuring the powder flow properties occurring in dynamic systems, such as powder mixers and screw conveyors. In this study, the rheological behaviour of powders at high shear rates has been evaluated by the ball indentation method. The technique, which simply consists of dropping a ball onto a cylindrical bed of previously consolidated powder, directly measures the material hardness, which is related to the unconfined yield stress by the constraint factor. The impact of the ball on the bed is recorded with a high-speed camera to determine velocity and penetration depth. The hardness against the strain rate is considered for four different materials. Because of their difference in particle size, and by using a range of drop heights and a range of indenter densities, the intermediate regime of flow has been fully analyzed. Although hardness is constant in the quasi-static condition, it results to be strain rate dependent in the intermediate regime of flow. Finally, a predictive correlation that allows the operator to choose the best operating conditions for achieving the desired flow regime is proposed, and the unconfined yield strength of the materials is inferred. [Display omitted] •Characterization of powder flowability in dynamic condition by ball indentation.•Pros and cons of dynamic ball indentation technique are discussed.•In the quasi-static regime of flow hardness is independent of the shear rate.•An increase in hardness with the shear rate is observed in the intermediate regime.