Synthesis, Single Crystal Structure and Characterization of N-Benzylmethylammonium Trifluoromethanesulfonate

The title compound, C 9 H 12 NO 3 F 3 S, was synthesized and characterized by elemental analyses, IR spectroscopy, thermogravimetric analysis and single crystal X-ray diffraction. The crystals are monoclinic, space group P 2 1 / c , Z = 4, The structure is stabilized by N–H···O and C–H···F hydrogen-...

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Bibliographic Details
Published in:Crystallography reports 2019-12, Vol.64 (7), p.1062-1065
Main Authors: Li, Shi-Geng, He, Guang-Hua, Li, Tao-Tao, Long, Bai-Hua
Format: Article
Language:English
Subjects:
Crystal structure
Crystallography and Scattering Methods
Hydrogen bonds
Infrared analysis
Infrared spectroscopy
Physics
Physics and Astronomy
Single crystals
Structural analysis
Structure of Organic Compounds
Thermogravimetric analysis
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Summary:The title compound, C 9 H 12 NO 3 F 3 S, was synthesized and characterized by elemental analyses, IR spectroscopy, thermogravimetric analysis and single crystal X-ray diffraction. The crystals are monoclinic, space group P 2 1 / c , Z = 4, The structure is stabilized by N–H···O and C–H···F hydrogen-bonds forming a three-dimensional network.
ISSN:1063-7745
1562-689X
DOI:10.1134/S1063774519070083