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Synthesis and application of carboxyethylthiosuccinic acid by thiol-ene click reaction: as a novel rust remover with corrosion inhibition properties
Carboxyethylthiosuccinic acid (CETSA) was synthesized by thiol-ene click reaction and determined by various characterization methods, such as 1 H NMR, IR and TG. A novel rust remover with corrosion inhibition was prepared by using CETSA as the main component. The results of rust removal were tested...
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| Published in: | Journal of chemical sciences (Bangalore, India) India), 2020-12, Vol.132 (1), Article 56 |
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| Main Authors: | , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c316t-35fb9d6370b75c3225ba1e4b3faf67409c1a76ac6595d1fe41dad2a481237f043 |
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| cites | cdi_FETCH-LOGICAL-c316t-35fb9d6370b75c3225ba1e4b3faf67409c1a76ac6595d1fe41dad2a481237f043 |
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| container_issue | 1 |
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| container_title | Journal of chemical sciences (Bangalore, India) |
| container_volume | 132 |
| creator | Gao, Huajing Xie, Ning Zhang, Jianxin Sun, Jian Zhang, Jianlin Jin, Zhaohui |
| description | Carboxyethylthiosuccinic acid (CETSA) was synthesized by thiol-ene click reaction and determined by various characterization methods, such as
1
H NMR, IR and TG. A novel rust remover with corrosion inhibition was prepared by using CETSA as the main component. The results of rust removal were tested by the difference method and intuitive comparison method, and its rust removal mechanism was explored. The corrosion inhibition effect of the composite reagent for A3 steel in 1 M HCl solution was investigated by static weight loss test, the adsorption isotherm was calculated and fitted.
Graphic abstract
CETSA was synthesized as a novel rust remover, which removed rust from the metal surface through penetration and chelation. It has excellent rust removal performance and protects the metal from corrosion by forming the adsorption membrane. |
| doi_str_mv | 10.1007/s12039-020-1756-9 |
| format | article |
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1
H NMR, IR and TG. A novel rust remover with corrosion inhibition was prepared by using CETSA as the main component. The results of rust removal were tested by the difference method and intuitive comparison method, and its rust removal mechanism was explored. The corrosion inhibition effect of the composite reagent for A3 steel in 1 M HCl solution was investigated by static weight loss test, the adsorption isotherm was calculated and fitted.
Graphic abstract
CETSA was synthesized as a novel rust remover, which removed rust from the metal surface through penetration and chelation. It has excellent rust removal performance and protects the metal from corrosion by forming the adsorption membrane.</description><identifier>ISSN: 0974-3626</identifier><identifier>EISSN: 0973-7103</identifier><identifier>DOI: 10.1007/s12039-020-1756-9</identifier><language>eng</language><publisher>New Delhi: Springer India</publisher><subject>Adsorption ; Chelation ; Chemical reactions ; Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Corrosion ; Corrosion effects ; Corrosion inhibitors ; Corrosion mechanisms ; Metal surfaces ; NMR ; Nuclear magnetic resonance ; Reagents ; Regular Article ; Rusting ; Weight loss</subject><ispartof>Journal of chemical sciences (Bangalore, India), 2020-12, Vol.132 (1), Article 56</ispartof><rights>Indian Academy of Sciences 2020</rights><rights>Indian Academy of Sciences 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-35fb9d6370b75c3225ba1e4b3faf67409c1a76ac6595d1fe41dad2a481237f043</citedby><cites>FETCH-LOGICAL-c316t-35fb9d6370b75c3225ba1e4b3faf67409c1a76ac6595d1fe41dad2a481237f043</cites><orcidid>0000-0001-5182-1632</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>Gao, Huajing</creatorcontrib><creatorcontrib>Xie, Ning</creatorcontrib><creatorcontrib>Zhang, Jianxin</creatorcontrib><creatorcontrib>Sun, Jian</creatorcontrib><creatorcontrib>Zhang, Jianlin</creatorcontrib><creatorcontrib>Jin, Zhaohui</creatorcontrib><title>Synthesis and application of carboxyethylthiosuccinic acid by thiol-ene click reaction: as a novel rust remover with corrosion inhibition properties</title><title>Journal of chemical sciences (Bangalore, India)</title><addtitle>J Chem Sci</addtitle><description>Carboxyethylthiosuccinic acid (CETSA) was synthesized by thiol-ene click reaction and determined by various characterization methods, such as
1
H NMR, IR and TG. A novel rust remover with corrosion inhibition was prepared by using CETSA as the main component. The results of rust removal were tested by the difference method and intuitive comparison method, and its rust removal mechanism was explored. The corrosion inhibition effect of the composite reagent for A3 steel in 1 M HCl solution was investigated by static weight loss test, the adsorption isotherm was calculated and fitted.
Graphic abstract
CETSA was synthesized as a novel rust remover, which removed rust from the metal surface through penetration and chelation. It has excellent rust removal performance and protects the metal from corrosion by forming the adsorption membrane.</description><subject>Adsorption</subject><subject>Chelation</subject><subject>Chemical reactions</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Corrosion</subject><subject>Corrosion effects</subject><subject>Corrosion inhibitors</subject><subject>Corrosion mechanisms</subject><subject>Metal surfaces</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Reagents</subject><subject>Regular Article</subject><subject>Rusting</subject><subject>Weight loss</subject><issn>0974-3626</issn><issn>0973-7103</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp1kMtOxCAYhRujiePoA7gjcY1yacvgzky8JZO4UNeEUmoZO1CBqn0PH1hqTVy54of_fOeQk2WnGJ1jhNhFwARRDhFBELOihHwvWyDOKGQY0f2fOYe0JOVhdhTCFiG6yhldZF-Po42tDiYAaWsg-74zSkbjLHANUNJX7nPUsR272BoXBqWMNQpIZWpQjWB67KC2GqjEvQKvpZrgSyCTIbDuXXfADyGmzS5dPPgwsQXKee_CFGJsayrzk9d712sfjQ7H2UEju6BPfs9l9nxz_bS-g5uH2_v11QYqissIadFUvC4pQxUrFCWkqCTWeUUb2ZQsR1xhyUqpyoIXNW50jmtZE5mvMKGsQTldZmezb4p-G3SIYusGb1OkSArGEOF8lVR4Vqn05-B1I3pvdtKPAiMxlS_m8kUqX0zlC54YMjMhae2L9n_O_0Pf2T-LLg</recordid><startdate>20201201</startdate><enddate>20201201</enddate><creator>Gao, Huajing</creator><creator>Xie, Ning</creator><creator>Zhang, Jianxin</creator><creator>Sun, Jian</creator><creator>Zhang, Jianlin</creator><creator>Jin, Zhaohui</creator><general>Springer India</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0001-5182-1632</orcidid></search><sort><creationdate>20201201</creationdate><title>Synthesis and application of carboxyethylthiosuccinic acid by thiol-ene click reaction: as a novel rust remover with corrosion inhibition properties</title><author>Gao, Huajing ; Xie, Ning ; Zhang, Jianxin ; Sun, Jian ; Zhang, Jianlin ; Jin, Zhaohui</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-35fb9d6370b75c3225ba1e4b3faf67409c1a76ac6595d1fe41dad2a481237f043</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Adsorption</topic><topic>Chelation</topic><topic>Chemical reactions</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Corrosion</topic><topic>Corrosion effects</topic><topic>Corrosion inhibitors</topic><topic>Corrosion mechanisms</topic><topic>Metal surfaces</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Reagents</topic><topic>Regular Article</topic><topic>Rusting</topic><topic>Weight loss</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gao, Huajing</creatorcontrib><creatorcontrib>Xie, Ning</creatorcontrib><creatorcontrib>Zhang, Jianxin</creatorcontrib><creatorcontrib>Sun, Jian</creatorcontrib><creatorcontrib>Zhang, Jianlin</creatorcontrib><creatorcontrib>Jin, Zhaohui</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of chemical sciences (Bangalore, India)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gao, Huajing</au><au>Xie, Ning</au><au>Zhang, Jianxin</au><au>Sun, Jian</au><au>Zhang, Jianlin</au><au>Jin, Zhaohui</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and application of carboxyethylthiosuccinic acid by thiol-ene click reaction: as a novel rust remover with corrosion inhibition properties</atitle><jtitle>Journal of chemical sciences (Bangalore, India)</jtitle><stitle>J Chem Sci</stitle><date>2020-12-01</date><risdate>2020</risdate><volume>132</volume><issue>1</issue><artnum>56</artnum><issn>0974-3626</issn><eissn>0973-7103</eissn><abstract>Carboxyethylthiosuccinic acid (CETSA) was synthesized by thiol-ene click reaction and determined by various characterization methods, such as
1
H NMR, IR and TG. A novel rust remover with corrosion inhibition was prepared by using CETSA as the main component. The results of rust removal were tested by the difference method and intuitive comparison method, and its rust removal mechanism was explored. The corrosion inhibition effect of the composite reagent for A3 steel in 1 M HCl solution was investigated by static weight loss test, the adsorption isotherm was calculated and fitted.
Graphic abstract
CETSA was synthesized as a novel rust remover, which removed rust from the metal surface through penetration and chelation. It has excellent rust removal performance and protects the metal from corrosion by forming the adsorption membrane.</abstract><cop>New Delhi</cop><pub>Springer India</pub><doi>10.1007/s12039-020-1756-9</doi><orcidid>https://orcid.org/0000-0001-5182-1632</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0974-3626 |
| ispartof | Journal of chemical sciences (Bangalore, India), 2020-12, Vol.132 (1), Article 56 |
| issn | 0974-3626 0973-7103 |
| language | eng |
| recordid | cdi_proquest_journals_2377702998 |
| source | Full-Text Journals in Chemistry (Open access); Springer Nature |
| subjects | Adsorption Chelation Chemical reactions Chemistry Chemistry and Materials Science Chemistry/Food Science Corrosion Corrosion effects Corrosion inhibitors Corrosion mechanisms Metal surfaces NMR Nuclear magnetic resonance Reagents Regular Article Rusting Weight loss |
| title | Synthesis and application of carboxyethylthiosuccinic acid by thiol-ene click reaction: as a novel rust remover with corrosion inhibition properties |
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