Quantitation of Si, B, Ca, Mg, Ba, and Zr in Complex-Alloyed Nickel Alloys by ICP-MS

The possibility of the use of a collision and reaction cell is shown and the optimum parameters for its adjustment are selected for the determination of Si, B, Ca, Mg, Ba, and Zr in a complex-alloyed nickel alloy via inductively coupled plasma mass spectrometry (ICP-MS). The procedure of sample diss...

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Bibliographic Details
Published in:Moscow University chemistry bulletin 2020, Vol.75 (1), p.22-27
Main Authors: Alekseev, A. V., Yakimovich, P. V., Proskurnina, E. V.
Format: Article
Language:English
Subjects:
Alloying
Alloys
Barium
Calcium
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Inductively coupled plasma mass spectrometry
Magnesium
Mass spectrometry
Nickel alloys
Nickel base alloys
Silicon
Zirconium
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Summary:The possibility of the use of a collision and reaction cell is shown and the optimum parameters for its adjustment are selected for the determination of Si, B, Ca, Mg, Ba, and Zr in a complex-alloyed nickel alloy via inductively coupled plasma mass spectrometry (ICP-MS). The procedure of sample dissolution and its preparation for the analysis is presented. The correctness of the obtained results is confirmed by the analysis of the certified reference standard of a nickel alloy.
ISSN:0027-1314
1935-0260
DOI:10.3103/S0027131420010022