Alkyl 3-Nitroacrylates in Reactions with Semicarbazide

The reactions of alkyl-3-nitroacrylates with semicarbazide as representative of polynitrogen nucleophiles proceeds at room temperature in a solution of glacial acetic acid and leads to aza-Michael adducts. Their structure was proved by 1 H, 13 C{ 1 H} NMR and IR spectroscopy methods.

Saved in:
Bibliographic Details
Published in:Russian journal of general chemistry 2020-03, Vol.90 (3), p.493-494
Main Authors: Pelipko, V. V., Adyukov, I. S., Baichurin, R. I., Makarenko, S. V.
Format: Article
Language:English
Subjects:
Acetic acid
Adducts
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Infrared spectroscopy
NMR
Nuclear magnetic resonance
Nucleophiles
Room temperature
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:The reactions of alkyl-3-nitroacrylates with semicarbazide as representative of polynitrogen nucleophiles proceeds at room temperature in a solution of glacial acetic acid and leads to aza-Michael adducts. Their structure was proved by 1 H, 13 C{ 1 H} NMR and IR spectroscopy methods.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363220030251