Synthesis of 4,4'-Bis[3-(Fluorodinitromethyl)-1H-1,2,4-triazol-5-Yl]azofurazan

A three-step method was developed for converting both ethoxycarbonylmethyl groups of 4,4'-bis[3-(ethoxycarbonylmethyl)-1 Н -1,2,4-triazol-5-yl]azofurazan into fluorodinitromethyl groups, enabling the preparation of the target 4,4'-bis[3-(fluorodinitromethyl)-1 Н -1,2,4-triazol-5-yl]azofura...

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Published in:Chemistry of heterocyclic compounds (New York, N.Y. 1965) N.Y. 1965), 2020-05, Vol.56 (5), p.619-622
Main Authors: Aleksandrova, Nataly S., Monogarov, Konstantin A., Sheremetev, Aleksei B.
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Language:English
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Chemistry
Chemistry and Materials Science
Combustion
Organic Chemistry
Pharmacy
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description A three-step method was developed for converting both ethoxycarbonylmethyl groups of 4,4'-bis[3-(ethoxycarbonylmethyl)-1 Н -1,2,4-triazol-5-yl]azofurazan into fluorodinitromethyl groups, enabling the preparation of the target 4,4'-bis[3-(fluorodinitromethyl)-1 Н -1,2,4-triazol-5-yl]azofurazan in 74% overall yield.
doi_str_mv 10.1007/s10593-020-02709-1
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Chemistry and Materials Science
Combustion
Organic Chemistry
Pharmacy
title Synthesis of 4,4'-Bis[3-(Fluorodinitromethyl)-1H-1,2,4-triazol-5-Yl]azofurazan
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