Synthesis and characterization of (E)-2-(1-hydrazonoethyl)-4,5-dimethylphenol from 2-hydroxy-4,5-dimethylacetophenone

This study reports the development of a novel substituted hydrazone prepared from 2-hydroxy-4,5-dimethylacetophenone and hydrazine in alkaline medium at controlled conditions which yields as corresponding hydrazone [(E)-2-(1-hydrazonoethyl)-4,5-dimethylphenol]. The structure of synthesized (E)-2-(1-...

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Bibliographic Details
Published in:Journal of chemical sciences (Bangalore, India) India), 2020-12, Vol.132 (1), Article 88
Main Authors: Gagare, Dinkar, Patil, Raju, Lokhande, Rama, Dwivedi, Poonam, Deshmukh, Ajay
Format: Article
Language:English
Subjects:
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
High performance liquid chromatography
Hydrazines
Hydrazones
Infrared analysis
NMR
Nuclear magnetic resonance
Regular Article
Spectrum analysis
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Summary:This study reports the development of a novel substituted hydrazone prepared from 2-hydroxy-4,5-dimethylacetophenone and hydrazine in alkaline medium at controlled conditions which yields as corresponding hydrazone [(E)-2-(1-hydrazonoethyl)-4,5-dimethylphenol]. The structure of synthesized (E)-2-(1-hydrazonoethyl)-4,5-dimethylphenol was elucidated by elemental analysis and spectroscopic techniques like infrared spectroscopy, ultraviolet–visible spectroscopy, high-performance liquid chromatography, proton nuclear magnetic resonance and mass spectrum.
ISSN:0974-3626
0973-7103
DOI:10.1007/s12039-020-01802-4