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Eddy current technique as a nondestructive method for evaluating the degree of sensitization of 304 stainless steel

•Using DL-EPR to evaluate %DOS of 304 SS sensitized in different conditions.•Characterizing the microstructure of sensitized samples.•Using eddy current technique to establish the relation between %DOS and ECT results.•Developing the equation of % DOS = 2×10-5(EC Voltage)2 −0.1031 (EC Voltage) + 120...

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Published in:Corrosion science 2020-08, Vol.173, p.108742, Article 108742
Main Authors: Kelidari, Yeganeh, Kashefi, Mehrdad, Mirjalili, Mostafa, Seyedi, Mahla, Krause, Thomas W.
Format: Article
Language:English
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Summary:•Using DL-EPR to evaluate %DOS of 304 SS sensitized in different conditions.•Characterizing the microstructure of sensitized samples.•Using eddy current technique to establish the relation between %DOS and ECT results.•Developing the equation of % DOS = 2×10-5(EC Voltage)2 −0.1031 (EC Voltage) + 120.95.•Developing the equation of % DOS = 178.48 (N.I.) + 177.01 between impedance and %DOS. The application of eddy current (EC) technique in detection of sensitization before the occurrence of intergranular corrosion was investigated. For this purpose, EC experiments were performed on 304 stainless-steels sensitized at 650 °C and 750 °C for 1–20 hours. The double-loop electrochemical potentiodynamic reactivation (DL-EPR) and microstructural investigations were also carried out to evaluate the degree of sensitization (DOS). The DL-EPR results showed that the maximum sensitivity occurred within 4 h at 650 °C. The EC results indicated a reduction in voltage and impedance with increasing DOS. Finally, empirical relationships between DL-EPR and EC test results were developed.
ISSN:0010-938X
1879-0496
DOI:10.1016/j.corsci.2020.108742