O-Trimethylsilyl-N-phenylsulfonylacetimidate: Synthesis and Structure

A method for silylation of N -acetylbenzenesulfonamide has been proposed. The structural features of the obtained O -trimethylsilyl- N -phenylsulfonylacetimidate have been studied by means of NMR and IR spectroscopy as well as single-crystal X-ray diffraction analysis.

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Bibliographic Details
Published in:Russian journal of general chemistry 2020-09, Vol.90 (9), p.1641-1645
Main Authors: Nikonov, A. Yu, Sterkhova, I. V., Kolyvanov, N. A., Serykh, V. Yu, Lazareva, N. F.
Format: Article
Language:English
Subjects:
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Crystals
Infrared spectroscopy
NMR
Nuclear magnetic resonance
Nuclear magnetic resonance spectroscopy
Single crystals
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Description
Summary:A method for silylation of N -acetylbenzenesulfonamide has been proposed. The structural features of the obtained O -trimethylsilyl- N -phenylsulfonylacetimidate have been studied by means of NMR and IR spectroscopy as well as single-crystal X-ray diffraction analysis.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363220090091