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Quantitative phase analysis and microstructural characterization of Portland cement blends with diatomite waste using the Rietveld method
This paper aims at giving new insights into the impacts of the particle sizes of diatomite waste on the hydration properties of Portland cement from the perspective of quantitative analysis using Rietveld refinements method. XRD identification coupled with Rietveld quantitative phase analysis, as we...
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Published in: | Journal of materials science 2021, Vol.56 (2), p.1242-1254 |
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description | This paper aims at giving new insights into the impacts of the particle sizes of diatomite waste on the hydration properties of Portland cement from the perspective of quantitative analysis using Rietveld refinements method. XRD identification coupled with Rietveld quantitative phase analysis, as well as isothermal calorimetry and SEM observation, was performed. The results show that the cement hydration during the induction period does not show any significant differences with the decrease in the sizes of the diatomite waste particles; however, hydration during the acceleration period was significantly enhanced. Finer diatomite waste particles (d50 |
doi_str_mv | 10.1007/s10853-020-05429-1 |
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XRD identification coupled with Rietveld quantitative phase analysis, as well as isothermal calorimetry and SEM observation, was performed. The results show that the cement hydration during the induction period does not show any significant differences with the decrease in the sizes of the diatomite waste particles; however, hydration during the acceleration period was significantly enhanced. Finer diatomite waste particles (d50 < 1070.9 nm) result in a significant increase in the amounts of ettringite (AFt) and calcium hydroxide (CH) during acceleration period of the cement. Moreover, diatomite waste incorporation contributes to accelerate the early formation of monosulfate (AFm); however, the formation of the AFm was not favorable as the sizes of the diatomite waste particles decrease. The improvement on the hydration of the Portland cement was largely affected by the particle sizes effects of the diatomite waste at the very early stage, and then by the reactivity of diatomite waste at the later stage.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-020-05429-1</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Analysis ; Calorimetry ; Cement ; Cement hydration ; Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Classical Mechanics ; Crystallography and Scattering Methods ; Diatomaceous earth ; Ettringite ; Hydration ; Materials Science ; Methods ; Polymer Sciences ; Portland cements ; Quantitative analysis ; Rietveld method ; Slaked lime ; Solid Mechanics</subject><ispartof>Journal of materials science, 2021, Vol.56 (2), p.1242-1254</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020</rights><rights>COPYRIGHT 2021 Springer</rights><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c431t-c14e2ce4e0784d4d460f7bc8654388c1d3653aab1fd4f95f9ded3c32b93c9dd13</citedby><cites>FETCH-LOGICAL-c431t-c14e2ce4e0784d4d460f7bc8654388c1d3653aab1fd4f95f9ded3c32b93c9dd13</cites><orcidid>0000-0001-6704-7661</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Liu, Runqing</creatorcontrib><creatorcontrib>Yang, Yuanquan</creatorcontrib><creatorcontrib>Zhao, Xingke</creatorcontrib><creatorcontrib>Pang, Bo</creatorcontrib><title>Quantitative phase analysis and microstructural characterization of Portland cement blends with diatomite waste using the Rietveld method</title><title>Journal of materials science</title><addtitle>J Mater Sci</addtitle><description>This paper aims at giving new insights into the impacts of the particle sizes of diatomite waste on the hydration properties of Portland cement from the perspective of quantitative analysis using Rietveld refinements method. XRD identification coupled with Rietveld quantitative phase analysis, as well as isothermal calorimetry and SEM observation, was performed. The results show that the cement hydration during the induction period does not show any significant differences with the decrease in the sizes of the diatomite waste particles; however, hydration during the acceleration period was significantly enhanced. Finer diatomite waste particles (d50 < 1070.9 nm) result in a significant increase in the amounts of ettringite (AFt) and calcium hydroxide (CH) during acceleration period of the cement. Moreover, diatomite waste incorporation contributes to accelerate the early formation of monosulfate (AFm); however, the formation of the AFm was not favorable as the sizes of the diatomite waste particles decrease. The improvement on the hydration of the Portland cement was largely affected by the particle sizes effects of the diatomite waste at the very early stage, and then by the reactivity of diatomite waste at the later stage.</description><subject>Analysis</subject><subject>Calorimetry</subject><subject>Cement</subject><subject>Cement hydration</subject><subject>Ceramics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Classical Mechanics</subject><subject>Crystallography and Scattering Methods</subject><subject>Diatomaceous earth</subject><subject>Ettringite</subject><subject>Hydration</subject><subject>Materials Science</subject><subject>Methods</subject><subject>Polymer Sciences</subject><subject>Portland cements</subject><subject>Quantitative analysis</subject><subject>Rietveld method</subject><subject>Slaked lime</subject><subject>Solid Mechanics</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kdtqVTEQhoMouK2-gFcBr7xYbU7rdFmKh0JBrXodspPJXilrJ9tkVmt9A9-62S5BeiMDyTB8fzIzPyGvOTvljPVnhbOhlQ0TrGGtEmPDn5ANb3vZqIHJp2TDmBCNUB1_Tl6UcsMYa3vBN-T3l8VEDGgw3AI9TKYANdHM9yWUmji6DzangnmxuGQzUzuZbCxCDr-qJkWaPP2cMs5H2MIeItLtDNEVehdwoi4YTPuAQO9MqedSQtxRnIBeB8BbmOsXgFNyL8kzb-YCr_7eJ-T7-3ffLj42V58-XF6cXzVWSY6N5QqEBQWsH5Sr0THfb-3QtUoOg-VOdq00Zsu9U35s_ejASSvFdpR2dI7LE_JmffeQ048FCuqbtOQ6ctFC9bzjrBNjpU5Xamdm0CH6hHXsGg7qRlIEH2r9vJNjOyol-yp4-0hQGYSfuDNLKfry6_VjVqzscbUlg9eHHPYm32vO9NFPvfqpq5_6j5_62LdcRaXCcQf5X9__UT0A5Iml0A</recordid><startdate>2021</startdate><enddate>2021</enddate><creator>Liu, Runqing</creator><creator>Yang, Yuanquan</creator><creator>Zhao, Xingke</creator><creator>Pang, Bo</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0001-6704-7661</orcidid></search><sort><creationdate>2021</creationdate><title>Quantitative phase analysis and microstructural characterization of Portland cement blends with diatomite waste using the Rietveld method</title><author>Liu, Runqing ; Yang, Yuanquan ; Zhao, Xingke ; Pang, Bo</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c431t-c14e2ce4e0784d4d460f7bc8654388c1d3653aab1fd4f95f9ded3c32b93c9dd13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Analysis</topic><topic>Calorimetry</topic><topic>Cement</topic><topic>Cement hydration</topic><topic>Ceramics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Classical Mechanics</topic><topic>Crystallography and Scattering Methods</topic><topic>Diatomaceous earth</topic><topic>Ettringite</topic><topic>Hydration</topic><topic>Materials Science</topic><topic>Methods</topic><topic>Polymer Sciences</topic><topic>Portland cements</topic><topic>Quantitative analysis</topic><topic>Rietveld method</topic><topic>Slaked lime</topic><topic>Solid Mechanics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Runqing</creatorcontrib><creatorcontrib>Yang, Yuanquan</creatorcontrib><creatorcontrib>Zhao, Xingke</creatorcontrib><creatorcontrib>Pang, Bo</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Runqing</au><au>Yang, Yuanquan</au><au>Zhao, Xingke</au><au>Pang, Bo</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Quantitative phase analysis and microstructural characterization of Portland cement blends with diatomite waste using the Rietveld method</atitle><jtitle>Journal of materials science</jtitle><stitle>J Mater Sci</stitle><date>2021</date><risdate>2021</risdate><volume>56</volume><issue>2</issue><spage>1242</spage><epage>1254</epage><pages>1242-1254</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><abstract>This paper aims at giving new insights into the impacts of the particle sizes of diatomite waste on the hydration properties of Portland cement from the perspective of quantitative analysis using Rietveld refinements method. XRD identification coupled with Rietveld quantitative phase analysis, as well as isothermal calorimetry and SEM observation, was performed. The results show that the cement hydration during the induction period does not show any significant differences with the decrease in the sizes of the diatomite waste particles; however, hydration during the acceleration period was significantly enhanced. Finer diatomite waste particles (d50 < 1070.9 nm) result in a significant increase in the amounts of ettringite (AFt) and calcium hydroxide (CH) during acceleration period of the cement. Moreover, diatomite waste incorporation contributes to accelerate the early formation of monosulfate (AFm); however, the formation of the AFm was not favorable as the sizes of the diatomite waste particles decrease. The improvement on the hydration of the Portland cement was largely affected by the particle sizes effects of the diatomite waste at the very early stage, and then by the reactivity of diatomite waste at the later stage.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10853-020-05429-1</doi><tpages>13</tpages><orcidid>https://orcid.org/0000-0001-6704-7661</orcidid></addata></record> |
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subjects | Analysis Calorimetry Cement Cement hydration Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Classical Mechanics Crystallography and Scattering Methods Diatomaceous earth Ettringite Hydration Materials Science Methods Polymer Sciences Portland cements Quantitative analysis Rietveld method Slaked lime Solid Mechanics |
title | Quantitative phase analysis and microstructural characterization of Portland cement blends with diatomite waste using the Rietveld method |
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