Synthesis, Molecular, and Crystal Structure of Tris(2-carbamoylmethoxyphenyl)phosphine Oxide

New tripodal ligand, tris(2-carbamoylmethoxyphenyl)phosphine oxide, has been synthesized via the alkylation of tris(2-hydroxyphenyl)phosphine oxide with chloroacetamide. The ligand structure has been studied by means of IR and NMR ( 1 H, 31 P) spectroscopy as well as X-ray diffraction.

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Bibliographic Details
Published in:Russian journal of general chemistry 2020-10, Vol.90 (10), p.1840-1844
Main Authors: Baulina, T. V., Kudryavtsev, I. Yu, Artem’ev, A. V., Bagryanskaya, I. Yu, Pasechnik, M. P., Brel, V. K.
Format: Article
Language:English
Subjects:
Alkylation
Chemical synthesis
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Crystal structure
Crystals
Infrared spectroscopy
Ligands
Molecular structure
NMR
Nuclear magnetic resonance
Phosphine oxide
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Description
Summary:New tripodal ligand, tris(2-carbamoylmethoxyphenyl)phosphine oxide, has been synthesized via the alkylation of tris(2-hydroxyphenyl)phosphine oxide with chloroacetamide. The ligand structure has been studied by means of IR and NMR ( 1 H, 31 P) spectroscopy as well as X-ray diffraction.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363220100059