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Ecofriendly synthesis, crystal chemistry, electrical, and low-temperature magnetic properties of nano-particles (Li–Cr) for drug delivery and MRI applications
Mixed Li (0.5− x /2) Fe (2.5− x /2) Cr x O 4 ( X = 0.0, 0.2, 0.4, 0.6, 0.8, 1.0) nano-ferrite system was synthesized by using Citrate gel auto-combustion method. Structural parameters such as lattice constant, hopping length, and X-ray density were reported and discussed with composition. The surfa...
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| Published in: | Journal of materials science. Materials in electronics 2021, Vol.32 (2), p.1392-1401 |
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| Main Authors: | , , , , , |
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| cited_by | cdi_FETCH-LOGICAL-c319t-9767a193fa5652da347a576cb52ef3be75d3d784ed6d6e9324393cba1c17cce33 |
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| cites | cdi_FETCH-LOGICAL-c319t-9767a193fa5652da347a576cb52ef3be75d3d784ed6d6e9324393cba1c17cce33 |
| container_end_page | 1401 |
| container_issue | 2 |
| container_start_page | 1392 |
| container_title | Journal of materials science. Materials in electronics |
| container_volume | 32 |
| creator | Ravinder, D. Nayak, D. Ravinder Rapolu, Sridhar Batoo, Khalid Mujasam Raslan, Emad H. Hadi, Mohammad |
| description | Mixed Li
(0.5−
x
/2)
Fe
(2.5−
x
/2)
Cr
x
O
4
(
X
= 0.0, 0.2, 0.4, 0.6, 0.8, 1.0) nano-ferrite system was synthesized by using Citrate gel auto-combustion method. Structural parameters such as lattice constant, hopping length, and X-ray density were reported and discussed with composition. The surface morphology was presented and explained with TEM analysis and SAED patterns. XRD patterns show the prepared samples are single-phase cubic spinel structure and the average particle size lies between 17 to 27 nm. TEM analysis shows prepared sample are the crystallite formation in nano-size. DC electrical properties presented variation with temperature and composition were discussed and studied well behind the Curie temperature. Magnetic measurements are carryout with VSM (Vibrating Sample Magnetometer), Observations have shown that magnetic properties are strongly influenced due to the substitution of Cr
3+
in Lithium ferrites. Two samples Li
0.5
Cr
0.6
Fe
1.9
O
4
and Li
0.5
Cr
1.0
Fe
1.5
O
4
were subjected to an applied field of 100 Oe between 5 and 375 K temperature for ZFC and FC (Zero Field Cooled and Field Cooled) measurements of magnetization which indicated blocking temperature at around 350 K for both samples beyond which they exhibited super-paramagnetic behavior. |
| doi_str_mv | 10.1007/s10854-020-04908-0 |
| format | article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2491441567</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2491441567</sourcerecordid><originalsourceid>FETCH-LOGICAL-c319t-9767a193fa5652da347a576cb52ef3be75d3d784ed6d6e9324393cba1c17cce33</originalsourceid><addsrcrecordid>eNp9kc2KFDEQx4O44LjrC3gKeFGYuPnsdB9lWHVhRBAFbyGTVM9myaTbJLPSN99hX8Bn80mMO4I3T0UV_4-CH0LPGX3NKNWXhdFeSUI5JVQOtCf0EVoxpQWRPf_6GK3ooDSRivMn6Gkpt5TSTop-hX5euWnMAZKPCy5LqjdQQlljl5dSbcTuBg6h1LysMURwNQdn4xrb5HGcvpMKhxmyrccM-GD3CWpweM5TO9YABU8jTjZNZLZtd7FdXm7Drx_3m_wKj1PGPh_32EMMd5CXh9QPn66xnefYemqYUrlAZ6ONBZ79nefoy9urz5v3ZPvx3fXmzZY4wYZKBt1pywYxWtUp7q2Q2irduZ3iMIodaOWF170E3_kOBsGlGITbWeaYdg6EOEcvTrnt-29HKNXcTsecWqXhcmBSMtXppuInlctTKRlGM-dwsHkxjJo_JMyJhGkkzAMJQ5tJnEylidMe8r_o_7h-A-oLkCs</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2491441567</pqid></control><display><type>article</type><title>Ecofriendly synthesis, crystal chemistry, electrical, and low-temperature magnetic properties of nano-particles (Li–Cr) for drug delivery and MRI applications</title><source>Springer Nature</source><creator>Ravinder, D. ; Nayak, D. Ravinder ; Rapolu, Sridhar ; Batoo, Khalid Mujasam ; Raslan, Emad H. ; Hadi, Mohammad</creator><creatorcontrib>Ravinder, D. ; Nayak, D. Ravinder ; Rapolu, Sridhar ; Batoo, Khalid Mujasam ; Raslan, Emad H. ; Hadi, Mohammad</creatorcontrib><description>Mixed Li
(0.5−
x
/2)
Fe
(2.5−
x
/2)
Cr
x
O
4
(
X
= 0.0, 0.2, 0.4, 0.6, 0.8, 1.0) nano-ferrite system was synthesized by using Citrate gel auto-combustion method. Structural parameters such as lattice constant, hopping length, and X-ray density were reported and discussed with composition. The surface morphology was presented and explained with TEM analysis and SAED patterns. XRD patterns show the prepared samples are single-phase cubic spinel structure and the average particle size lies between 17 to 27 nm. TEM analysis shows prepared sample are the crystallite formation in nano-size. DC electrical properties presented variation with temperature and composition were discussed and studied well behind the Curie temperature. Magnetic measurements are carryout with VSM (Vibrating Sample Magnetometer), Observations have shown that magnetic properties are strongly influenced due to the substitution of Cr
3+
in Lithium ferrites. Two samples Li
0.5
Cr
0.6
Fe
1.9
O
4
and Li
0.5
Cr
1.0
Fe
1.5
O
4
were subjected to an applied field of 100 Oe between 5 and 375 K temperature for ZFC and FC (Zero Field Cooled and Field Cooled) measurements of magnetization which indicated blocking temperature at around 350 K for both samples beyond which they exhibited super-paramagnetic behavior.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-020-04908-0</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Characterization and Evaluation of Materials ; Chemical synthesis ; Chemistry and Materials Science ; Composition ; Crystallites ; Curie temperature ; Electrical properties ; Lattice parameters ; Lithium ferrite ; Low temperature ; Magnetic measurement ; Magnetic properties ; Magnetism ; Magnetometers ; Materials Science ; Morphology ; Nanoparticles ; Optical and Electronic Materials</subject><ispartof>Journal of materials science. Materials in electronics, 2021, Vol.32 (2), p.1392-1401</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2021</rights><rights>Springer Science+Business Media, LLC, part of Springer Nature 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-9767a193fa5652da347a576cb52ef3be75d3d784ed6d6e9324393cba1c17cce33</citedby><cites>FETCH-LOGICAL-c319t-9767a193fa5652da347a576cb52ef3be75d3d784ed6d6e9324393cba1c17cce33</cites><orcidid>0000-0002-0626-3034</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Ravinder, D.</creatorcontrib><creatorcontrib>Nayak, D. Ravinder</creatorcontrib><creatorcontrib>Rapolu, Sridhar</creatorcontrib><creatorcontrib>Batoo, Khalid Mujasam</creatorcontrib><creatorcontrib>Raslan, Emad H.</creatorcontrib><creatorcontrib>Hadi, Mohammad</creatorcontrib><title>Ecofriendly synthesis, crystal chemistry, electrical, and low-temperature magnetic properties of nano-particles (Li–Cr) for drug delivery and MRI applications</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>Mixed Li
(0.5−
x
/2)
Fe
(2.5−
x
/2)
Cr
x
O
4
(
X
= 0.0, 0.2, 0.4, 0.6, 0.8, 1.0) nano-ferrite system was synthesized by using Citrate gel auto-combustion method. Structural parameters such as lattice constant, hopping length, and X-ray density were reported and discussed with composition. The surface morphology was presented and explained with TEM analysis and SAED patterns. XRD patterns show the prepared samples are single-phase cubic spinel structure and the average particle size lies between 17 to 27 nm. TEM analysis shows prepared sample are the crystallite formation in nano-size. DC electrical properties presented variation with temperature and composition were discussed and studied well behind the Curie temperature. Magnetic measurements are carryout with VSM (Vibrating Sample Magnetometer), Observations have shown that magnetic properties are strongly influenced due to the substitution of Cr
3+
in Lithium ferrites. Two samples Li
0.5
Cr
0.6
Fe
1.9
O
4
and Li
0.5
Cr
1.0
Fe
1.5
O
4
were subjected to an applied field of 100 Oe between 5 and 375 K temperature for ZFC and FC (Zero Field Cooled and Field Cooled) measurements of magnetization which indicated blocking temperature at around 350 K for both samples beyond which they exhibited super-paramagnetic behavior.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemical synthesis</subject><subject>Chemistry and Materials Science</subject><subject>Composition</subject><subject>Crystallites</subject><subject>Curie temperature</subject><subject>Electrical properties</subject><subject>Lattice parameters</subject><subject>Lithium ferrite</subject><subject>Low temperature</subject><subject>Magnetic measurement</subject><subject>Magnetic properties</subject><subject>Magnetism</subject><subject>Magnetometers</subject><subject>Materials Science</subject><subject>Morphology</subject><subject>Nanoparticles</subject><subject>Optical and Electronic Materials</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kc2KFDEQx4O44LjrC3gKeFGYuPnsdB9lWHVhRBAFbyGTVM9myaTbJLPSN99hX8Bn80mMO4I3T0UV_4-CH0LPGX3NKNWXhdFeSUI5JVQOtCf0EVoxpQWRPf_6GK3ooDSRivMn6Gkpt5TSTop-hX5euWnMAZKPCy5LqjdQQlljl5dSbcTuBg6h1LysMURwNQdn4xrb5HGcvpMKhxmyrccM-GD3CWpweM5TO9YABU8jTjZNZLZtd7FdXm7Drx_3m_wKj1PGPh_32EMMd5CXh9QPn66xnefYemqYUrlAZ6ONBZ79nefoy9urz5v3ZPvx3fXmzZY4wYZKBt1pywYxWtUp7q2Q2irduZ3iMIodaOWF170E3_kOBsGlGITbWeaYdg6EOEcvTrnt-29HKNXcTsecWqXhcmBSMtXppuInlctTKRlGM-dwsHkxjJo_JMyJhGkkzAMJQ5tJnEylidMe8r_o_7h-A-oLkCs</recordid><startdate>2021</startdate><enddate>2021</enddate><creator>Ravinder, D.</creator><creator>Nayak, D. Ravinder</creator><creator>Rapolu, Sridhar</creator><creator>Batoo, Khalid Mujasam</creator><creator>Raslan, Emad H.</creator><creator>Hadi, Mohammad</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope><orcidid>https://orcid.org/0000-0002-0626-3034</orcidid></search><sort><creationdate>2021</creationdate><title>Ecofriendly synthesis, crystal chemistry, electrical, and low-temperature magnetic properties of nano-particles (Li–Cr) for drug delivery and MRI applications</title><author>Ravinder, D. ; Nayak, D. Ravinder ; Rapolu, Sridhar ; Batoo, Khalid Mujasam ; Raslan, Emad H. ; Hadi, Mohammad</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-9767a193fa5652da347a576cb52ef3be75d3d784ed6d6e9324393cba1c17cce33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemical synthesis</topic><topic>Chemistry and Materials Science</topic><topic>Composition</topic><topic>Crystallites</topic><topic>Curie temperature</topic><topic>Electrical properties</topic><topic>Lattice parameters</topic><topic>Lithium ferrite</topic><topic>Low temperature</topic><topic>Magnetic measurement</topic><topic>Magnetic properties</topic><topic>Magnetism</topic><topic>Magnetometers</topic><topic>Materials Science</topic><topic>Morphology</topic><topic>Nanoparticles</topic><topic>Optical and Electronic Materials</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ravinder, D.</creatorcontrib><creatorcontrib>Nayak, D. Ravinder</creatorcontrib><creatorcontrib>Rapolu, Sridhar</creatorcontrib><creatorcontrib>Batoo, Khalid Mujasam</creatorcontrib><creatorcontrib>Raslan, Emad H.</creatorcontrib><creatorcontrib>Hadi, Mohammad</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central</collection><collection>Advanced Technologies & Aerospace Database (1962 - current)</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>ProQuest advanced technologies & aerospace journals</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials science collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ravinder, D.</au><au>Nayak, D. Ravinder</au><au>Rapolu, Sridhar</au><au>Batoo, Khalid Mujasam</au><au>Raslan, Emad H.</au><au>Hadi, Mohammad</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Ecofriendly synthesis, crystal chemistry, electrical, and low-temperature magnetic properties of nano-particles (Li–Cr) for drug delivery and MRI applications</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2021</date><risdate>2021</risdate><volume>32</volume><issue>2</issue><spage>1392</spage><epage>1401</epage><pages>1392-1401</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>Mixed Li
(0.5−
x
/2)
Fe
(2.5−
x
/2)
Cr
x
O
4
(
X
= 0.0, 0.2, 0.4, 0.6, 0.8, 1.0) nano-ferrite system was synthesized by using Citrate gel auto-combustion method. Structural parameters such as lattice constant, hopping length, and X-ray density were reported and discussed with composition. The surface morphology was presented and explained with TEM analysis and SAED patterns. XRD patterns show the prepared samples are single-phase cubic spinel structure and the average particle size lies between 17 to 27 nm. TEM analysis shows prepared sample are the crystallite formation in nano-size. DC electrical properties presented variation with temperature and composition were discussed and studied well behind the Curie temperature. Magnetic measurements are carryout with VSM (Vibrating Sample Magnetometer), Observations have shown that magnetic properties are strongly influenced due to the substitution of Cr
3+
in Lithium ferrites. Two samples Li
0.5
Cr
0.6
Fe
1.9
O
4
and Li
0.5
Cr
1.0
Fe
1.5
O
4
were subjected to an applied field of 100 Oe between 5 and 375 K temperature for ZFC and FC (Zero Field Cooled and Field Cooled) measurements of magnetization which indicated blocking temperature at around 350 K for both samples beyond which they exhibited super-paramagnetic behavior.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-020-04908-0</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0002-0626-3034</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0957-4522 |
| ispartof | Journal of materials science. Materials in electronics, 2021, Vol.32 (2), p.1392-1401 |
| issn | 0957-4522 1573-482X |
| language | eng |
| recordid | cdi_proquest_journals_2491441567 |
| source | Springer Nature |
| subjects | Characterization and Evaluation of Materials Chemical synthesis Chemistry and Materials Science Composition Crystallites Curie temperature Electrical properties Lattice parameters Lithium ferrite Low temperature Magnetic measurement Magnetic properties Magnetism Magnetometers Materials Science Morphology Nanoparticles Optical and Electronic Materials |
| title | Ecofriendly synthesis, crystal chemistry, electrical, and low-temperature magnetic properties of nano-particles (Li–Cr) for drug delivery and MRI applications |
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